4.12
Section 4
Pinnacle PcX OPeratiOn
Pinnacle Operators Manual
Pickering Laboratories Inc.
Click Add Method.
Type a Name for your method. For this example, type “Tutorial”, and click OK.
The Pinnacle PCX software has now added the method “Tutorial” to the list of available methods. Highlight this
method if it is not already done so.
Under Initial Settings Tab, type:
Run Time, min: 60
Equilibration Time, min: 5
Column t, °C: 38
Column Type: 1154150 Na cation exchange
Reactor t, °C: 36
Reactor Volume, ml: 0.5
Pump 1 Flow rate, ml/min: 0.3
Reagent 1: Hypochlorite
Pump 2 Flow rate, ml/min: 0.3
Reagent 2: OPA
Click on the Pumps Tab, then click once in the box under Time. The cursor should now be flashing here. Type in
your desired Times and flow rates below. Use the Add button to add lines to the table. Use the data from the table
below as a guide. Time is the elapsed time in minutes. P1 and P2 are the flow rates of each pump in ml/min.
Time, min P1, ml/min P2, ml/min
1.0 0.3 0.5
1.6 0.8 0.0
3.8 1.0 0.05
12.5 0.0 0.05
30 0.1 0.0
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