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2690
Waters 2690 User Manual
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Qu
ic
k S
u
mma
r
y
The figure below
sum
mar
izes
the inf
o
r
mation contained in this Quic
k Star
t Guide. Use it
as a
ref
eren
ce af
ter you have read the
entire
docum
ent.
Start
Power on the
Separat
ions
Module
Prime the Solvent
Management
System
Prime
t
he Pl
unger
Seal W
ash Pump
(If In
s
talle
d)
The Funct
ion
Begins
t
o
Run
Configu
re the
Separat
ions
Module
Degas or
Sparge
Eluents
Purge the Sampl
e
Mana
gement
Syste
m
Adjust
the
Seal Pack
Prime t
he Needle
Wa
s
h P
u
m
p
Load the
Carouse
l
s
Ye
s
No
Perform
a
n Au
tomat
ic
Run?
Set Con
t
rol
Switc
hes
Set Flo
w Rate and
Co
mpos
it
ion
Set Sparge Rat
e
(if Appli
c
able)
Pre
ss
Direct
Func
ti
on
Screen Key
Selec
t Direct
Functi
on to Perfor
m
Enter Fun
ction
Paramete
rs
Press th
e
Run
Sampl
es
Screen Key
on the
Main S
creen
Enter
Dat
a Requi
r
e
d by
the Separ
ation Method,
Samp
le Set, or
Sample T
emplate
The Run Ends as
Progr
ammed
Select t
he Separati
on
Method,
Sample Set, or
T
emplate t
o
Run,
then
Press
Run
Screen Key
Press t
he
Routine
Screen Key to St
art
th
e Ru
n
2
4
Table of Contents
Quick Summary
3
Notes and Warnings
4
Conventions Used in this Guide
4
Introduction
5
Before You Begin
5
System Description
6
Waters 2690 XE Separations Module (Front View)
6
Preparing the Separations Module for Operation
7
Powering on
7
Startup Diagnostics
7
Diagnostic Test Results Screen
7
The Main Screen
8
Configuring the Separations Module
9
No Interaction Mode
9
System Controller Mode
9
Controlled by Millennium
10
Controlled by Masslynx Mode
11
Controlled by Millennium 2.XX Mode
11
Controlled by Operate Gradient by Event in
12
Controlled Via RS-232 (ASCII) or (Binary) Modes
13
Setting Report Options
13
Programming for Auto Shutdown
14
Report Options Dialog Box
14
To Enable the Auto Shutdown Function
15
Auto-Shutdown Dialog Box
15
Preparing the Solvent Management System
17
Degassing Solvents
17
In-Line Vacuum Degassing
17
Preparing the Solvent Management System for Operation
17
Status Screen
18
Sparging
19
Programmed Sparge Dialog Box
19
Priming the Solvent Management System
20
Dry Prime
20
Prime/Vent Valve with Syringe
20
Dry Prime Dialog Box
21
Wet Prime
22
To Perform a Wet Prime
22
Wet Prime Dialog Box
22
Equilibrating Solvents the Vacuum Degasser
23
Priming the Plunger Seal Wash Pump
23
To Prime the Plunger Seal Wash Pump
23
Diagnostics Screen
24
Preparing the Sample Management System
25
Purging the Sample Management System
25
Preparing the Sample Management System for Operation
25
Priming the Needle-Wash Pump
26
Purge Injector Dialog Box
26
Selecting a Needle-Wash Solvent
27
Suggested Needle Wash Solvents
27
Adjusting the Seal Pack
27
To Prime the Needle-Wash Pump
27
Loading Vials
28
Carousel Codes and Colors
28
Loading the Carousel
28
To Load the Carousels
29
Door Is Open Dialog Box
29
Performing a Direct Control Run
30
Setting up a Direct Control Run
30
First Page of Status Screen
31
Second Page of Status Screen
31
Status Screen Parameters
32
To Access the Direct Control Functions
34
Direct Functions Menu
34
Making Automatic Runs
36
System Controller or no Interaction Mode
36
Controlled by Millennium Chromatography Manager Modes
36
Making Automatic Runs in Stand-Alone Mode
37
Making an Automatic Run in a Stand-Alone Configuration
37
Running a Sample Set
38
To Run a Sample Set in a Standalone Mode
38
Icons in the Run Samples Screen
38
Sample Set Screen – Functional View
39
Making a Run from a Sample Template
40
Run Samples Screen with Solvents Required Dialog Box
40
Modifying a Sample Set During a Run
41
Performing a Stat Run
41
Setup Dialog Box
41
Editing a Separation Method
42
Importing and Exporting Methods
42
Importing Methods
42
To Perform a Stat Run While a Sample Set Is Running
42
Exporting Methods
43
Import Methods Screen
43
Methods Screen
44
Export Methods Screen
44
Making Automatic Runs under Millennium Control
45
Making a Run Using Millennium Software
45
Making an Automatic Run Using Masslynx Software
46
Stopping a Run
47
Before Powering off
48
Powering off
48
To Power off the Separations Module
48
Recommended Preparation Procedures
49
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Waters 2690 Specifications
General
Brand
Waters
Model
2690
Category
Control Unit
Language
English
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