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Hanna Instruments HI931 - User Manual

Hanna Instruments HI931
218 pages
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MANUALS
AUTOMATIC
POTENTIOMETRIC TITRATOR
HI931

Table of Contents

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Hanna Instruments HI931 Specifications

General IconGeneral
BrandHanna Instruments
ModelHI931
CategoryLaboratory Equipment
LanguageEnglish

Summary

Introduction and Safety

How to Find Information

Guides users to different sections of the manual for information.

Safety Measures

Lists essential safety precautions to follow during instrument operation.

Titrator Connections Overview

Front View Connections

Illustrates and labels the connections on the front of the titrator.

Rear View Connections

Illustrates and labels the connections on the rear of the titrator.

User Interface Description

Keypad Layout and Function

Details the titrator's keypad, categorizing keys by function.

Display Screen Information

Explains the user interface and the information displayed on the screen.

Getting Started with the Titrator

Language Selection

Instructions on how to change the titrator's display language.

Contextual Help Usage

Explains how to access contextual help screens for assistance.

Methods Management

Covers standard and user-defined methods for analysis.

pH Electrode Calibration

Details the preparation and procedure for pH electrode calibration.

Performing a Titration

Required Solutions and Materials

Lists the necessary reagents and water for performing a titration.

Burette Priming Procedure

Instructions for filling and preparing the burette with titrant.

Method Selection and Parameter Setting

Steps to select a titration method and configure its parameters.

Titration Process and Results

Setting Up Titration Reports

Customizing which data fields are included in the titration report.

Sample Preparation Steps

Detailed guide for preparing the sample in the titration beaker.

Executing and Understanding Titration

Steps to start titration and interpret displayed information.

Viewing and Managing Titration Data

Viewing Titration Graphs

How to view real-time titration graphs and adjust axis scales.

Titration Termination Conditions

Explains how titrations end and how the endpoint is marked.

Results Management

Viewing Last Titration Data

Steps to review the data from the most recent titration.

Printing Titration Reports

How to connect a printer and print titration reports.

Saving Data to USB

Instructions for saving titration or logging data onto a USB device.

Method Parameters for Titration

Pump and Dosing Configuration

Settings for pump configuration and dosing type (Linear/Dynamic).

End Point Mode and Recognition

Setting titration end point mode and recognition options.

Pre-Titration and Measurement Settings

Configuring pre-titration volume, stir time, and measurement mode.

Introduction to Titration Methods

Selecting Titration Methods

How to select and activate a titration method on the titrator.

Standard Methods Overview

Information on standard methods provided for common analyses.

Managing Titration Methods

Upgrading and Deleting Standard Methods

Procedures for upgrading or removing standard titration methods.

Restoring Standard Methods

Restoring all standard methods to their original factory settings.

User Method Creation and Deletion

Guide on creating and removing user-defined titration methods.

Method Options and Parameters

Viewing and Modifying Methods

How to view and modify parameters of existing titration methods.

Method Name and Revision

Setting or changing the name and revision number of a titration method.

Stirrer Configuration

Selecting the stirrer and setting its speed for a titration method.

Pump and Dosing Type Settings

Specifying pump and configuring dosing type (Linear/Dynamic).

End Point Mode and Determination

Configuring end point detection methods like Fixed or Equivalence point.

Recognition Options for Accuracy

Setting threshold, range, and filtered derivatives for accurate endpoint recognition.

Pre-Titration and Measurement Settings

Configuring pre-titration volume, stir time, and measurement mode.

Electrode Type and Blank Options

Specifying electrode type and blank calculation options.

Calculation Methods

Selecting standard titration, sample calculation, and standardization methods.

Titrant and Analyte Configuration

Setting titrant name, concentration, and analyte size.

Volume and Signal Settings

Setting maximum titrant volume, potential range, and signal averaging.

Significant Figures and Printing

Formatting result display and printing method parameters.

Running and Stopping a Titration

Starting and Suspending a Titration

Steps to initiate, pause, and resume a titration analysis.

Viewing Titration Curves

How to display and interpret titration curves during analysis.

Titration Termination Conditions

Explains the conditions that lead to the termination of a titration.

pH Measurement and Calibration

pH Mode Display and Options

Shows the pH mode display and lists available option keys.

pH Setup Configuration

Configuring settings for pH measurement and calibration.

pH Calibration Procedure

Information on when and why pH calibration is necessary.

Data Logging in pH Mode

Overview and customization of data logging in pH mode.

mV Measurement and Calibration

mV Mode Display and Options

Shows the mV mode display and lists available option keys.

mV Setup Configuration

Configuring settings for mV measurement.

Relative mV Calibration

Steps for performing relative mV calibration.

Data Logging in mV Mode

Overview and customization of data logging in mV mode.

ISE Measurement and Calibration

ISE Mode Display and Options

Shows the ISE mode display and lists available option keys.

ISE Setup Configuration

Configuring settings for ISE measurement and calibration.

ISE Calibration Process

Information on when and why ISE calibration is necessary.

Data Logging in ISE Mode

Overview and customization of data logging in ISE mode.

Auxiliary Burette Operations

Accessing Burette Menu

Accessing the burette menu for operations like priming.

Priming the Burette

Steps for filling and preparing the burette with titrant.

Rinse Tip and Manual Dispense

Dispensing small volumes to clear tip air or manually dispense titrant.

Purge Burette for Cleaning

Procedure for emptying the burette for cleaning or storage.

Results and Reports Management

Stirrer Control

Turning the stirrer on/off and adjusting its speed.

Reviewing Analysis Reports

Reviewing the last analysis report and all saved reports.

GLP Data and Meter Information

Displaying GLP data and titrator configuration details.

Customizing Reports

Customizing reports for pH, mV, ISE, and titration results.

Burette Maintenance Procedures

Burette Assembly and Changing

Description of the burette assembly and steps for changing it.

Disassembling and Reassembling Burette

Instructions for taking apart and putting back together the burette assembly.

Cleaning the Burette

Detailed procedure for cleaning the burette and its components.

Burette Preparation (Filling)

Steps for properly filling the burette with titrant before use.

Peripherals and Connectivity

Connecting to a Printer

How to connect a parallel printer to the titrator.

Connecting an External PC Keyboard

Connecting an external PC keyboard for easier input.

Connecting to a Computer (USB)

Connecting the titrator to a computer via USB for data transfer.

Technical Specifications

HI931 Specifications Overview

Detailed technical specifications for the HI931 titrator.

Connectivity and Additional Features

Details of connection ports and other product specifications.

Accessories Catalog

Titration Solutions and Buffers

List of pH calibration buffers and titration reagents.

Electrode Cleaning and Storage Solutions

Solutions for cleaning, storing, and refilling electrodes.

Sensors: Electrodes and Temperature Probe

List of available pH, ORP, half-cell, ISE, and temperature sensors.

Titrator Components Identification

Visual identification and part numbers of titrator components.

General Information and Support

Certification and Disposal

Conformance to CE directives and electrical equipment disposal guidelines.

User Recommendations and Safety

General advice on product suitability and safe use in environments.

Warranty and Service Information

Warranty details and contact information for service and repairs.

Specific Titration Methods

0.1 N Sodium Hydroxide Standardization

Method for standardizing 0.1N NaOH against Potassium Hydrogen Phthalate.

0.1 N Hydrochloric Acid Standardization

Method for standardizing 0.1N HCl against Sodium Hydroxide.

0.1 M Sodium Thiosulfate Standardization

Method for standardizing 0.1M Sodium Thiosulfate against Potassium Iodate.

0.02 M Silver Nitrate Titration

Method for standardizing 0.02M Silver Nitrate against Sodium Chloride.

Alkalinity of Water Analysis (pH 4.5)

Method for determining total alkalinity in water to pH 4.5.

Acidity of Water Analysis (pH 8.3)

Method for determining total (phenolphthalein) acidity in water to pH 8.3.

Chloride in Water Determination

Method for determining chloride concentration in water.

Neutralization with Sulfuric Acid

Method for determining base concentration by titration with sulfuric acid.

Neutralization with Sodium Hydroxide

Method for determining acid concentration by titration with sodium hydroxide.

Troubleshooting Procedures

Troubleshooting Dosing Accuracy (Large Dose)

Method for verifying dosing and signal accuracy using large dose dispensing.

Troubleshooting Temperature and mV Channels

Procedures to check temperature and mV channel logging and stability.

Troubleshooting Dosing Accuracy (Small Dose)

Method for verifying titrator dosing accuracy using small dose dispensing.

Troubleshooting Stirring Speed

Procedure to check the stirrer speed and propeller operation.

Titration Theory Fundamentals

General Review of Titration Theory

Introduction to titration principles, uses, and advantages/disadvantages.

Types of Titration by Method

Classifies titrations based on measurement methods like amperometric and potentiometric.

Types of Titration by Reaction

Categorizes titrations based on reaction types like acid-base and redox.

Titration Sequence Types

Discusses titrations classified by sequence, such as back and multiple endpoint titrations.

Titration Apparatus and Procedure

Details manual and automatic titration apparatus and typical procedures.

Titration Results and Sources of Error

Discusses accuracy, repeatability, and common sources of error in titrations.

Titration Calculations

Explains calculations for sample concentration and titrant standardization.

Glossary of Titration Terms

Definitions of key terms related to titration theory and practice.

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