Milestone DMA-80 evo

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Milestone Srl MA213-003 – DMA-80 EVO – User Manual

113

- BCE224i-1S parameters (Highlighted parameters are proper for the communication with DMA software)

Main Page

Table of Contents4
Safety Rules8
General Information8
Safety Rules for Start-Up8
Safety Rules in Operations8
Safety in Service Operations9
No Manipulation on the Unit Allowed9
Parts Replacement9
Customer Support9
Other Hints9
Safety of Operation9
Cleaning Instructions10
Maintenance Instructions10
Fuses10
Installation11
Unpacking and Checking List11
Evo Standard Equipment12
Catalyst and Amalgamator Installation15
Evo Setup22
Voltage Setting23
DMA Connection with Terminal 66026
DMA 80 EVO Connection with PC27
DMA Safety Switch31
Gas Connection31
Oxygen Tank32
Milestone Air Compressor32
Evo General Information36
Technical Data36
EVO Front View38
EVO Back View39
EVO Internal View39
Evo Milestone Connect41
Software45
Login45
Operation According to FDA-21 CFR Part 1145
Login According to CFR 1146
Methods Release by Signature46
Data File Storage and Signature46
Data Safety of Measurement File in CFR Part 1147
Documentation - Erroneous Login47
Password Expiration47
Program End/Logout47
General Operations Tips48
Popup Menu48
File Opening, Closing, Saving and Deleting48
Main Page DMA-80 EVO Software51
Print53
Automatic Printout in PDF55
Import CSV Files55
How to Import a CSV File55
Importing CSV Formatted Data into Excel57
Method Page59
Methods-Parameters60
Create a New Method62
Methods Management65
Calibration Page66
Calibration- Parameters66
Create a New Calibration71
How to Prepare Aqueous Standard Solutions78
Reference Page79
Measure Page83
Measurement- Parameters83
Create a New Measurement93
System Page95
System- Parameters96
Settings98
Settings-Access98
Settings-Settings103
Service122
Service-Autosampler123
Service-Detector126
Service-Test128
Maintenance130
Consumables Replacement130
Water Discharge from the Outlet Connection139
Sample Boat Cleaning140
Software Message and Inquiries141
Status Message141
Analytical Error Messages141
Technical Error Messages144
Tips & Techniques146
General Rules146
Calibration146
How to Make a Standard Liquid Solution146
How to Store a Liquid Standard Solution147
How to Store Standard Reference Materials147
Blanks147
How to Get Good Blanks147
Cleaning Methods148
Tips for a Good Cleaning148
Quality Control149
How to Set up a QC Program149
Acceptance Criteria for QC Samples149
Sample Processing150
Recommendations for Preservation of Samples150
How to Clean the DMA-80 Boats150
How to Work at Ultratrace Levels151
How to Work at Standard Levels (Ppb/Ppm)153
How to Increase the Reproducibility155
How to Work with Unknown Samples155
How to Work with Non-Homogeneous Samples155
How to Increase the Recovery of Difficult Samples156
How to Work with Difficult Matrices156
How to Work with Liquid Samples in Auto-Sampler Mode, in Order to Avoid Evaporation157
Conditioning Procedure for New Catalyst Tube158
Introduction158
21Cfr-11 Dma Software159
Activation of the 21CFR Part 11159
Overview of User Profiles and Access Levels160
Declaration of Compliance "DMA Software" with FDA-21CFR Part 11163
Safety Data Sheet169

Milestone DMA-80 evo - Page 115

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