Pickering Laboratories Pinnacle PCX - Page 122

6.3-9
Section 6
ApplicAtions
Pinnacle Operators Manual
Pickering Laboratories Inc.
METHOD 4: 1846150 C
18
COLUMN (4.6X150 MM) WITH AQUEOUS SAMPLES
COLUMN TEMP: 42 ºC HPLC FLOW RATE: 1.0ML/MIN REAGENT FLOW RATE: 0.3ML/MIN
CONDITIONS FOR AQUEOUS SAMPLES
Time (Min) Water % MeOH %
0 100 0
1 100 0
1.1 88 12
26 30 70
26.1 0 100
28 0 100
28.1 100 0
38 100 0
105 15 20 25 30
0
min
1
2
3
4
5
6
7
8
9
10
11
12
4 ng of Carbamates in 150 µL