Pickering Laboratories Pinnacle PCX - Page 123

6.3-10
Section 6
ApplicAtions
Pinnacle Operators Manual
Pickering Laboratories Inc.
METHOD 5: 0846250 C
8
COLUMN (4.6X250MM) WITH METHANOLIC SAMPLES
HPLC FLOW RATE: 1.0ML/MIN COLUMN TEMPERATURE: 42˚ C REAGENT FLOW RATE: 0.3 ML/MIN
CONDITIONS FOR METHANOLIC SAMPLES
Time (Min) Water % MeOH %
0 85 15
1 85 15
44 25 75
44.1 0 100
49 0 100
49.1 85 15
57 85 15
Carbamate Test Mix, 2.5ppm, 10μl injection, 25cm, Carbamate C
8
Column (0846250)
5
100
1
2
3
4
15
20
25
30
35
40
min
5
6
7
8
9
10
11
12