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NORMALAB NDI 450 - Page 96

NORMALAB NDI 450
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NORMALAB France
2012
N O R M A L A B F r a n c e
96/118
Final boiling point
detection (FBP)
No detection or
divergent value
Verify that the modification of final heating
is not too great in relation to the declared
detection threshold.
Verify declared protection threshold.
Final volume
The final volume is not
correct
Verify the calibration of the test tube and its
declaration.
Ensure that the initial volume was correct.
Verify that the temperature of the test tube
compartment is correct (an increase in the
temperature expands the liquid and falsifies
measurement of the volume or evaporates
light distillate samples).
Verify the final residue.
Verify the leak tightness of the connection
stopper between the flask and silicone tube.
Verify the presence and efficacy of the
diaphragm on the test tube neck (case of
light distillate products).
The test tube has been cleaned and dried
before charging in the flask (error on drips
remaining in the test tube).
Poor calibration with a liquid generating a
convex meniscus (verify with level detector
on the sample).

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