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Rigaku Smartlab SE User Manual

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Smartlab
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Instruction Manual
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Rigaku Smartlab SE Specifications

General IconGeneral
BrandRigaku
ModelSmartlab SE
CategoryLaboratory Equipment
LanguageEnglish

Summary

Overview of SmartLab SE

Features of SmartLab SE

Horizontal Sample Mount Goniometer

Describes the theta-theta goniometer with horizontal sample mount for precise positioning.

Sample Section

Details the three units of the sample section: attachment platform, attachment, and sample holder.

X-ray Generator

Outlines the specifications of the X-ray generator, including load, voltage, and current ranges.

Cross Beam Optics (CBO)

Explains the CBO system for switching between divergent and parallel beams using selection slits.

Incident Optics Section

Describes the three units of the incident optics section for various beam geometries.

Receiving Optics Section

Details the six optical units for reducing background and improving resolution.

Detector

Introduces the D/teX Ultra250 1D detector and its capabilities for fast, high-resolution measurements.

Optics Switching System

Explains how SmartLab Studio II retains optics alignment results when switching optical devices.

Optical Device Detection

Describes how SmartLab Studio II checks and guides optical device configurations.

Control Software (SmartLab Studio II)

Integrates alignment, measurement, and analysis in one package for guided procedures.

Parts of the SmartLab SE

Main Unit

Identifies key components of the main unit, including PC, power key, and safety features.

Rear View of SmartLab SE

Shows and labels the rear panel connectors for power, cooling water, and control cables.

Goniometer Components

Details the parts of the goniometer: arms, optics sections, detector, and sample section.

Software Configuration Details

Control Software

Explains the XRD Measurement plugin for controlling the system and performing measurements.

Basic Data Processing

Describes the Data Manager plugin for performing basic data processing tasks.

Operational Procedures

Turning On and Off SmartLab SE

Procedure for safely powering on and off the SmartLab SE unit using the power key.

Opening and Closing the Door

Instructions for safely opening and closing the instrument door, considering safety interlocks.

Emergency Off Switch (EMO)

Describes the function and operation of the emergency off switch to cut power in urgent situations.

Optical Devices

Connecting and Removing Optical Device Cable

Guides on how to connect and disconnect optical device cables for system recognition.

Incident Optics Unit #1

Details the optical device for selecting incident beam type, including incident beam path.

CBO Unit Types

Explains various CBO units (Cu, E, α) for switching beam types, listing their applications.

Incident Optics Unit #2

Describes optical devices for conditioning incident X-ray beams, like Soller slits or monochromators.

Incident Slit

Slits installed on the theta_s arm to control beam divergence or width.

PB Collimator Adapter

Base for mounting collimators with parallel beams from multilayer mirrors or CBO-f.

Point Optics Unit

Used for measurements with point beams, added after switching to point focus.

Incident Attenuator

Used to adjust X-ray intensities at the incident side.

BB Collimator Adapter

Base for mounting BB collimator; Kβ filter can be inserted.

Incident Kβ Filter

Filter for the incident side to absorb Kβ X-rays, inserted into the BB collimator adapter.

Receiving Slit #1

Unit installed on theta_d arm to hold Kβ filter for diffracted beam.

Receiving Optics Unit #1

Adapter for installing parallel slit analyzers (PSA) parallel to the 2 theta direction.

Scattered Radiation Protector

Reduces scattered X-ray background, used with receiving slit box.

Receiving Optics Unit #2

Adapter for installing receiving Soller slits parallel to the theta_d axis divergence direction.

Receiving Slit #2

Functions as a virtual receiving slit, limiting detector area and controlling resolution.

Attenuator

Adjusts diffracted X-ray beam intensity using metal films on a rotating disc.

Detector Systems

D/teX Ultra250 Detector

Semi-conductor 1D detector for efficient, high-speed X-ray intensity detection and integration.

Detector Adapter (Detachable Type)

Adapter enabling attachment/detachment of D/teX Ultra250 with optional monochromator.

Diffracted Beam Monochromator (DBM)

Removes Kβ X-rays, enhances energy resolution for detecting minor component peaks.

DBM for D/teX OD BB

Monochromator for para-focusing optics to monochromatize diffracted beam to Ka X-rays.

DBM for D/teX OD BB/PB

Monochromator for Ka X-rays; angle adjustment for bent/flat geometry.

HyPix-400 Detector

Multi-dimensional semiconductor hybrid pixel array detector for high dynamic range and sensitivity.

Attachment Platform

Fixed and Universal Z Attachment Platforms

Platforms for fixing samples; universal Z allows Z-axis adjustment and various attachments.

Direct Beam Stop

Prevents direct X-ray beam from reaching the detector area during measurements.

Knife Edge

Effective in reducing backgrounds in 1D measurements with D/teX Ultra250.

Attachment Base

Mounting Attachment Base to Goniometer

Steps for installing attachment bases onto the universal Z attachment platform.

Standard Attachment Base

Used with attachment heads on the universal Z platform for powder/bulk samples.

β Attachment Base

Allows sample rotation (β) on the surface plane for averaging particle size variations.

φ Attachment Base

Enables control of rotational axis (φ) on the sample surface plane in micro angles.

Attachments

ASC-6/ASC-10 Attachment

Turret-based attachments for consecutive measurements of multiple samples.

αβ Attachment

Controls sample rotation (β) and tilt (α) for pole figure and stress measurements.

χφ Attachment

Controls sample rotation (φ) and tilt (χ) for thin film and pole figure measurements.

Multipurpose High Temperature Attachment

Maintains sample at high temperature for observing crystal structure/composition changes.

Corrosion Resistant High-Temperature Attachment Reactor-X

High-temperature attachment with infrared heater for rapid heating and stable temperature control.

DSC Attachment

Performs differential scanning calorimetry and XRD simultaneously during heating/cooling.

Anton Paar Attachment

Various attachments for temperature adjustment (HTK, XRK, TTK, CHC) with specific functions.

Attachment Heads

Mounting Attachment Head

Instructions on how to unlock, open clasps, align, and secure an attachment head.

Standard Attachment Head

Basic attachment head with no movable axes, used for powder and bulk samples.

RxRy Attachment Head

Features Rx and Ry axes for tilt adjustments, used for reflectivity and RSM measurements.

XY-20 mm Attachment Head

Provides +/-10 mm X/Y translation for micro area measurements.

XY-4 inch φ Attachment Head

Provides +/-50 mm X/Y translation for 4-inch wafer mapping.

Capillary Spin Attachment Head

Used to spin capillary-filled samples during measurements.

Battery Cell Attachment Head

Used for charging/discharging batteries during X-ray diffraction of electrode materials.

Anton Paar Attachment Head

Dome-shaped sample heating unit from Anton Paar for temperature control.

Sample Plates

Height Reference Sample Plate

Used with glass/aluminum holders for sample alignment, includes center slit and Si reference.

Transmission SAXS Sample Plate

Used for fibrous/film samples in transmission method, included with SAXS unit.

β Spin Sample Plate

Used with glass/aluminum holders and β attachment base for sample rotation.

Wafer Sample Plate and Sample Spacer

Plates and spacers for wafer-shaped samples, available in 4, 6, and 8-inch sizes.

Sample Holding Magnets

Used to secure samples up to 3 mm thick on sample plates.

Wafer Sample Plates

Lists available wafer sample plates (4, 6, 8-inch) and their combinations.

Sample Holders

Glass Sample Holder

Used for measuring powder samples.

Aluminum Sample Holder

Used for measuring powder or small bulk samples.

Low Background Sample Holder

Prevents sample holder diffraction X-rays, reducing halos for low angle measurements.

Transmission SAXS Sample Holder

Used for fibrous or film samples in transmission method, included with SAXS unit.

Capillary Holder

Mounts capillary samples onto the spin attachment head for rotation during measurement.

General-purpose Sample Holder

For reflection and transmission measurements of powder, fibrous, and film samples.

Air-sensitive Sample Holder

Places samples in a simple airtight condition during measurements.

Accessories

Accessory of Main Unit

Lists accessories for the main unit, including Kβ filter, beam stop, and sample holders.

Accessory of Fixed Sample Platform

Lists accessories for the fixed sample platform, including center slit and Si reference sample.

Accessory of Universal Z Attachment Platform

Lists accessories for the universal Z attachment platform, like sample plates and heads.

Example of Sample Mounting

Powder Sample Mounting

Describes filling powder into holders and inserting into fixed/height reference sample plates.

Bulk Sample Mounting

Mounting bulk samples using aluminum holders or wafer plates based on size.

Sample Mounting for Transmission SAXS

Mounting fibrous/film samples using transmission SAXS sample holder.

Wafer-shaped Samples Mounting

Using wafer plates and spacers for measuring wafer samples, including magnet usage.

Periodic Maintenance

Optics and Detector Maintenance

Re-adjustment requirements for multilayer mirrors, attenuators, and detectors.

Cooling Water Management

Guidance on checking and maintaining cooling water levels and replacement.

Cooling Water Filter Maintenance

Recommends periodic filter changes to prevent clogging and maintain water pressure.

Observation Window Care

Precautions for cleaning and maintaining the lead-content glass observation window.

Maintenance Parts List

Lists consumables like O-rings, silicone grease, X-ray tubes, and filters.

Troubleshooting Guide

Problem Resolution

Addresses issues like door locking, startup errors, goniometer stops, and generator stops.

Alarm Indicator and Alarm Sound Operations

Explains alarm patterns and sound cues for errors like XG or communication issues.

Column: X-ray Principles and Details

Characteristic X-rays

Explains the generation of continuous and characteristic X-ray spectra.

X-ray Spectrum of Cu Target

Illustrates the intensity vs. wavelength spectrum for a copper target.

Wavelengths of Characteristic X-rays

Lists wavelengths of characteristic X-rays for various target elements.

Tube Voltage and Tube Current

Discusses the relationship between tube parameters and X-ray intensity, and optimum settings.

Penetration Depth (Effective Thickness)

Provides formulas and tables to calculate effective sample thickness based on X-ray usage rate.

Cross Beam Optics (CBO) Explanation

Detailed explanation of CBO system, its types, and optical paths for beam switching.

Incident Monochromator Crystal

Describes Ge/Si crystals for X-ray monochromatization and their applications based on resolution.

Kβ Filter

Explains the function of Kβ filters and lists elements used as filters for different targets.

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