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Rigaku SmartLab User Manual

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Automated Multipurpose
X-ray Diffractomete
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Instruction Manual

Table of Contents

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Rigaku SmartLab Specifications

General IconGeneral
TypeX-ray Diffractometer
SoftwareSmartLab Studio II
X-ray SourceRotating anode
DetectorScintillation counter, hybrid pixel detector
Goniometer radius300 mm
X-ray generator3 kW
Optical configurationsparallel beam, focusing beam
ApplicationsPowder diffraction, thin film analysis, small angle X-ray scattering (SAXS), X-ray reflectivity (XRR)
GoniometerVertical goniometer

Summary

Product Features

High-accuracy theta-theta goniometer

Describes the precision goniometer for sample positioning and movement control.

X-ray generator

Explains the high-intensity rotating anode and sealed tube X-ray generators used.

Cross beam optics (CBO)

Covers the optical system for switching between divergent, parallel, and convergent beams.

Alignment mechanism (monochromators and analyzers)

Explains automatic adjustment mechanisms for monochromators and analyzers.

Receiving analyzer system

Describes systems for analyzing diffracted beams, including double-slit and parallel-slit analyzers.

Incident optics system

Details mechanisms for conditioning the incident X-ray beam.

Control software (SmartLab Guidance)

Introduces the primary software for controlling the system and performing measurements.

Names of Parts

Goniometer

Details the parts and function of the goniometer assembly.

X-ray tube

Describes the rotating anode and sealed tube X-ray sources.

Software Configuration

Control software

Describes the SmartLab Guidance software for system operation.

Turning On and Off SmartLab

Turning on SmartLab

Step-by-step instructions for powering on the SmartLab system.

Starting SmartLab Guidance

Guides on launching and logging into the SmartLab Guidance software.

Startup

Details the procedure for starting the measurement sequence.

Shutdown

Provides instructions for properly shutting down the SmartLab system.

Turning off SmartLab

Explains how to completely power off the SmartLab system.

Opening and Closing the Door

Opening the door

Steps to safely open the radiation enclosure door.

Closing the door

Steps to safely close the radiation enclosure door.

Emergency stop switch (EMO)

Explains the function and use of the emergency stop button.

Optics

Incident optics unit (standard incident optics unit)

Details the components for conditioning the incident X-ray beam.

Detector

Explains the function and types of detectors for X-ray measurement.

D/teX Ultra (option: 5741A300)

Describes the 1D detector for high-speed X-ray intensity detection.

PILATUS (option: 5742A101)

Details the PILATUS hybrid 2D detector.

Sample Stage

Attachments

Examples of Sample Mounting

Measurements

Preparing for measurements

Steps to prepare the system before starting measurements.

Setting the hardware configuration

Procedure for configuring the system's hardware components.

Selecting a Package Measurement

Guides on choosing pre-defined measurement protocols.

Periodic Maintenance

Optics maintenance

Maintenance tasks for optical components like mirrors and attenuators.

Troubleshooting

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