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Agilent Technologies 7200 User Manual
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90
Operation Manual
4
Operating in Chemical Ionization (CI) Mode
To Perform a CI Autotune
89
91
Table of Contents
Table of Contents
5
Introduction
10
Abbreviations Used
10
The 7200 Accurate-Mass Quadrupole Time-Of-Flight GC/MS System
12
Hardware Description
15
Important Safety Warnings
16
Safety and Regulatory Certifications
20
Intended Use
23
Cleaning/Recycling the Product
23
Liquid Spills
23
Moving or Storing the MS
23
Installing GC Columns
25
Columns
26
To Prepare a Capillary Column for Installation
29
To Install a Capillary Column in a Split/Splitless Inlet
31
To Condition a Capillary Column
33
To Install a Capillary Column in the GC/MS Interface
35
To Prepare the Column Ends for a CFT Fitting
38
Operating in Electron Impact (EI) Mode
44
Operating the MS from the Data System
44
The GC/MS Interface
45
Before You Turn on the MS
47
Pumping down
48
Controlling Temperatures
48
Controlling Column Flow
48
Controlling Collision Cell Flow
49
Venting the MS
50
Typical Vacuum Pressures in EI Mode
51
To Set Monitors for Temperature and Vacuum Status
52
To Set the MS Analyzer Temperature
55
To Set the GC/MS Interface Temperature from the Masshunter Workstation
57
To Calibrate the Column
58
To Configure the Collision Cell Gas
60
To Set the Collision Cell Gas Flow Rate
61
To Autotune the MS for EI Mode
62
To Remove the Upper RIS Cover
64
To Open the Analyzer Cover for Access to the Analyzer Sideplate
65
To Pump down the MS
66
To Vent the MS
69
Operating in Chemical Ionization (CI) Mode
72
Setting up Your MS to Operate in CI Mode
72
The CI GC/MS Interface
73
Operating the CI MS
75
High Vacuum Pressure in CI Mode
76
Other Reagent Gases
78
CI Autotune
80
The Flow Control Module
82
To Switch from the EI Mode to CI Mode
83
To Operate the Reagent Gas Flow Control Module
85
To Set a Reagent Gas Flow
87
To Perform a CI Autotune
88
Using the Removable Ion Source
92
The Removable Ion Source
92
To Change the Ion Source
94
To Install the RIS Probe Extraction Tool
97
To Remove the Source from the Analyzer Chamber
99
To Change the Ion Source on the RIS Probe Extraction Tool
101
To Install the Ion Source in the Analyzer Chamber
103
To Remove the RIS Probe Extraction Tool from the Instrument
104
General Maintenance
106
Before Starting
106
Maintaining the Vacuum System
111
Maintaining the Analyzer
112
To Disassemble the EI Ion Source
114
To Assemble the EI Ion Source
116
To Disassemble the CI Ion Source
118
To Assemble the CI Ion Source
120
To Clean the Ion Source
122
To Remove a Filament
126
To Install a Filament
128
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Agilent Technologies 7200 Specifications
General
Brand
Agilent Technologies
Model
7200
Category
Laboratory Equipment
Language
English
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