Proton Spectrum
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8 Proton Spectrum
This chapter describes the acquisition and processing of a one-dimensional 1H NMR
spectrum using the standard Bruker parameter set PROTON. The pulse sequence zg30 (see
figure below) consists of the recycling delay, the radio-frequency (RF) pulse, and the
acquisition time during which the signal is recorded. The pulse angle is shown to be 30
0
. The
two parameters, d1 and p1, correspond to the length of the recycle delay and the length of
the 90
0
RF pulse, respectively.
The time intervals depicted in the pulse sequence diagrams are not drawn to scale. For
example, d1 is typically a few seconds while p1 is typically a few microseconds in length.
The sample to be used is 30 mg of Menthyl Antranilate in DMSO-d6.
8.1 Experiment Setup
Create a new dataset
• On the menu bar, click Acquire | Create Dataset to open the Create New Dataset
window.
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