Safety
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2 Safety
In  terms  of  safety  the  presence  of  a  relatively  strong  magnet  is  what  differentiates  NMR
spectrometers from most other laboratory equipment. When designing an NMR laboratory, or
training  personnel  who  will  work  in  or  around  the  laboratory,  no  other  feature  is  of  greater
significance.  As  long  as  correct  procedures  are  adhered  to,  working  in  the  vicinity  of
superconducting magnets is completely safe and has no known harmful medical side effects.
Negligence however can result in serious accidents.
The magnet is potentially hazardous due to:
• The large attractive force it exerts on ferromagnetic objects.
• The large content of liquid nitrogen and helium.
2.1 Magnetic Safety
A magnetic field surrounds the magnet in all directions. This field (known as the stray field) is
invisible and supervisors should have posted warning signs at appropriate locations. Objects
made  of  ferromagnetic  materials,  e.g.  iron,  steel  etc.  will  be  attracted  to  the  magnet.  If  a
ferromagnetic  object  is  brought  too  close,  it  may  suddenly  be  drawn  into  the  magnet  with
surprising  force.  This  may  damage  the  magnet,  or  cause  personal  injury  to  anyone  in  the
way!
It is important that people working in the vicinity of the magnet fully understand the potential
hazards.  Of  critical  importance  is  that  people  fitted  with  cardiac  pacemakers  or  metallic
implants should never be allowed near the magnet.
Because  the  strength  of  the  stray  field  drops  significantly  as  one  moves  away  from  the
magnet, it is important to discuss worksite safety around magnets with your supervisor.
2.1.1 Cryogenic Safety
The magnet contains  relatively large quantities of  liquid helium and nitrogen.  These liquids,
referred to as cryogens, serve to keep the magnet core at a very low temperature.
Because  of the  very  low temperatures  involved,  gloves, a  long  sleeved  shirt  or  lab  coat
and  safety  goggles  should  always  be  worn  when  handling  cryogens.  Direct  contact  with
these liquids can cause frostbite. The system manager should regularly check and make sure
that evaporating gases are free to escape from the magnet, i.e. the release valves must not
be blocked. Do not attempt to refill the magnet with helium or nitrogen unless you have been
trained in the correct procedure.
Helium and nitrogen are non-toxic gases. However, because of a possible magnet quench,
whereupon  the  room  may  suddenly  fill  with  evaporated  gases,  adequate  ventilation  must
always be provided.
2.2 Electrical Safety
The  spectrometer  hardware  is  no  more  or  less  hazardous  than  any  typical  electronic  or
pneumatic hardware and should be treated accordingly. Do not remove any of the protective
panels from the  various units. They  are fitted to  protect  you and should  only be opened  by
qualified  service  personnel.  The  main  panel  at  the  rear  of  the  console  is  designed  to  be
removed  using  two  quick  release  screws,  but  again,  this  should  only  be  done  by  trained
personnel. Please note that, unless disconnected, cooling fans on the rear panel will continue
to run even with the panel removed.