Serinus 44 User Manual 3.0
Procedure
1. Open - Main Menu Calibration Menu.
2. Note down the current value for Conv. Efficiency NH3.
3. Edit - Conv. Efficiency NH3 - (change to 100%) - Accept.
4. Supply the instrument with a known concentration of NH
3
span gas at roughly 80% of the full-
scale monitoring range of the particular instrument. Label this value as [NH
3
]
SUPPLIED
.
5. Allow the instrument to achieve a prolonged, stable measurement response and note down the
NH
3
reading as shown on the instrument. Label this measurement as [NH
3
]
MEASURED
.
6. Use the noted measurements to calculate the converter efficiency using Equation 6.
7. If the converter efficiency is 80% or greater, the converter is working well, return the converter
efficiency to the original value. Adjustments to the converter efficiency value should only be
made based on a multipoint check (refer to Section 5.8.2). If the converter efficiency is outside of
this range, the test has failed and a multipoint converter efficiency adjustment should be
performed.
5.8.2 Multipoint NH
3
Converter Efficiency Adjustment
A multipoint converter efficiency check is performed to determine the actual converter efficiency
across the range of the instrument. Thus allowing the user to calculate a new converter efficiency
value that can be adjusted in the instrument.
In the S44, the Conv. Efficiency NH3 value displayed in the Main Menu Service Menu
Calculation Factors Menu encompasses losses from the external converter, the in-line NH
3
scrubber
and the second NO
2
to NO converter coil.
Note: For the following, the results for the NO and NO
2
and NO
X
channels can be ignored.
Equipment Required
Gas Dilution Calibrator (such as a Serinus Cal 1000/2000/3000).
NH
3
gas cylinder reference standard.
Zero Air Generator.
Procedure
1. Open - Main Menu Calibration Menu.
2. Note down the current value for Conv. Efficiency NH3.
3. Edit - Conv. Efficiency NH3 - (change to 100%) - Accept.
4. Supply the instrument with zero air from your gas dilution calibrator.
5. Allow the instrument to achieve a prolonged, stable measurement response and note down the
NH
3
value for reference only. If you get greater than 3 to 5 ppb you need to troubleshoot the
instrument and calibration system before continuing with this procedure.
6. Supply the instrument with a known concentration of NH
3
span gas at roughly 80% of the full-
scale monitoring range of the particular instrument. Label this value as [NH
3
]
SUPPLIED
.