Bruker AVANCE NEO - Page 4

Contents
iv H171804E_14_001
5.4.2 Probes Equipped with ATM Using the Manual Tuning Routine ........................................41
5.5 Spinning the Sample.........................................................................................................43
5.6 Shimming ..........................................................................................................................44
5.6.1 Routine Shimming Using TopShim ...................................................................................44
5.7 Setting the Probe/Solvent Dependent Parameters ...........................................................44
5.8 Adjusting the Receiver Gain .............................................................................................44
5.9 Starting the Acquisition .....................................................................................................44
5.10 Processing the Data..........................................................................................................45
6 Preparing for Acquisition, Frequency Related Parameters..........................................................47
6.1 Frequency .........................................................................................................................47
6.2 Numerical Explanation of Transmitted, Basic and Offset Frequencies.............................48
7 The NMR Sample ..............................................................................................................................51
7.1 Solvent Selection ..............................................................................................................51
7.2 Sample Tube.....................................................................................................................52
7.3 Sample Handling...............................................................................................................53
8 Proton Spectrum ..............................................................................................................................55
8.1 Experiment Setup .............................................................................................................55
8.2 Acquisition.........................................................................................................................59
8.3 Processing ........................................................................................................................59
8.4 Integration .........................................................................................................................61
8.5 Plotting the 1D Proton Spectra .........................................................................................63
8.6 Optimizing the Sweep Width.............................................................................................64
9 ¹³C Spectrum with Proton Decoupling............................................................................................67
9.1 Experiment Setup .............................................................................................................68
9.2 Acquisition.........................................................................................................................70
9.3 Processing ........................................................................................................................70
9.4 Peak Picking .....................................................................................................................72
9.5 Plotting the 1D Carbon Spectrum .....................................................................................73
10 Contact ..............................................................................................................................................75
List of Figures...................................................................................................................................77
List of Tables ....................................................................................................................................79
Glossary ............................................................................................................................................81
Index ..................................................................................................................................................83