Proton Spectrum
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• Enable Show Recommended to get the list of the most common small molecule
experiments.
• Ensure that the source directory is
<Topspin>\exp\stan\nmr\par
and not
<Topspin>\exp\stan\nmr\par\user
• In the table select PROTON as experiment and click Set selected item in editor.
• In the Create New Dataset window check Set solvent and in the drop-down list select
DMSO.
• In the TITLE field enter a text stating the experiment, sample, the solvent and any other
useful information. The title information can be used to search for a dataset.
• In the New Dataset window, click OK.
• On the menu bar, click Acquire.
To acquire a spectrum, use the Workflow buttons in the Workflow button bar from left to right
(see steps below). Alternatively, commands which are displayed in brackets of the various
popup windows, can also be typed at the TopSpin command prompt (e.g. ej, ij, edte etc.).
• On the Sample button, click the drop-down arrow to see more options.
• In the list, select Eject sample manually (ej).
Wait until the sample lift air is turned on and remove the sample which may be in the
magnet.
Load the sample
• Place the sample with the spinner onto the top of the magnet.
• On the Sample button, click the drop-down arrow to see more options.
• In the list, select Insert sample manually (ij).
Wait until the sample is lowered down into the probe and the lift air is turned off. A clicking
sound may be heard.
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