Bruker VANTEC-1 - Page 90

Calibration VÅNTEC-1 Detector User Manual
7 - 2 M88-E01072
Table 7.1 – Parameters for Quartz standard reference
Table 7.2 – Parameters for NIST 1976 standard reference
Goniometer Divergent slit Generator
settings
Scan
parameters
Scan speed
Radiation Theta/Theta Theta/2-theta Variable Fixed
(mm)
Kβ filter kV mA Increment PSD
(sec)
Scintillation
(step/sec)
Cr 20.03 20.03 20.03 40.06 0.3° 0.6 V 35 45 .006 30 .002
Co 15.52 15.52 15.52 31.04 0.3° 0.6 Fe 35 45 .006 30 .002
Cu 13.32 13.32 13.32 26.64 0.3° 0.6 Ni 40 40 .006 30 .002
Goniometer Divergent slit Generator
settings
Scan
parameters
Scan speed
Radiation Theta/Theta Theta/2-theta Variable Fixed
(mm)
Kβ filter kV mA Increment PSD
(sec)
Scintillation
(step/sec)
Cr 26.67 26.67 26.67 53.34 0.3° 0.6 V 35 45 .006 30 .002
Co 20.52 20.52 20.52 41.05 0.3° 0.6 Fe 35 45 .006 30 .002
Cu 17.57 17.57 17.57 35.15 0.3° 0.6 Ni 40 40 .006 30 .002