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MKC-710
KEM MKC-710 User Manual
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8. Troub
leshootin
g
98
Drift level is too high
8-3.
START
Are joints greased?
Is septum new?
Repair by
manufacturer
END
Apply grease
Change with new one
NO
NO
YES
Is reagent correct?
YES
Use correct reagent
NO
YES
Is reagent new?
Change with new one
NO
YES
Is inner burette dry?
Dry the burette
NO
Is anode in conta
ct
with diaphragm?
Use anode adjuster to d
etach
from each other 1.5
~2.0
mm
NO
YES
YES
Inner burette or
Electrode good?
Change it if malfunctioning
NO
YES
107
109
Table of Contents
Table of Contents
7
Preparations for Measurement
11
Supplied Parts
11
Installation and Start-Up
14
Assembly of Titration Cell
14
Installation of Clamp Filter
15
Power Cable
16
Installation of Solvent Change Unit（Option
17
Installation of Manual Solvent Change Unit
17
Installation of Auto Solvent Change Unit
19
Parts Configuration and each Function
23
Appearance and Name
23
Key Functions (General)
26
Basic Key Operation
27
Description of Display Messages
28
Setting Language
29
Setting Date and Time
30
Basic Operation
31
Sequence of Measurement
31
Assemble the Titration Cell
32
Filling Reagent and Draining
33
Catholyte
33
Anolyte
34
Measure the Sample
37
Re-Calculate Titration Data
39
Batch Processing of Titration Data
41
Read Data, Store in USB Flash Drive
43
Saving Method Conditions, Setting up on PC
45
Method
46
Titration Parameter
49
Calculation Parameter
54
Calculation Formula
57
Report Parameter
59
Function Tools
62
Function
62
Manual Operation
62
Data File
63
Method
65
Data Copy
65
History
66
Sample
66
Reagent
68
Bromine Number and Index
69
Preparation of Reagent
70
Measurement Procedure
71
Balance Setting
72
Connecting USB Devices
74
Connecting Android Devices
75
Connecting to Instrument
75
Starting App
76
Starting Pre-Titration
77
Starting Measurement
78
Measurement
80
Entering Weight
80
Uninstall Android Apps
81
Setup
82
Interface
83
RS-232C Setting
83
Date Acquisition Software (SOFT-CAP)
84
Printer Setting
84
Balance Setting
86
USB Setting
86
Operator
87
Date＆Time
88
Serial no
89
LCD Contrast
89
Language
90
Beep
91
Parameter Clear
92
Other
93
Maintenance
94
Daily Maintenance
94
Karl Fischer Grease
94
Replacement of Septum
95
Changing the Desiccant
95
Replacement of the Anolyte (Anode Reagent)
96
Replacement of the Catholyte (Cathode Reagent)
96
Check the Instrument
97
Check the Cable
97
Check the Connectors
97
Other Maintenance
98
Storage of the Instrument
98
Cleaning the Electrode
98
Cleaning the Titration Cell
101
Distance Adjustment between Anode Electrode and Diaphragm
101
Replacement of Pump Tube
102
Replacement of the Filter
103
Replacing the Clock Battery
104
Troubleshooting
105
Error Messages and Alarm Messages
105
Stirrer Does Not Work Properly
107
Drift Level Is too High
108
It Runs into Over-Titration
109
Poor Repeatability or no EP Found
110
Glass Contact Area Jammed
111
When the Drain Pump Is Clogged
112
Others
113
Parts List
113
Options
117
Specification
122
Principle of Measurement
123
Karl Fischer Reagent
124
Parameter List
127
Setup Parameters
127
Method Parameters
129
Selection of Method Parameters and Printout
130
International Standards
131
Warranty and After-Sales Service
132
4
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KEM MKC-710 Specifications
General
Brand
KEM
Model
MKC-710
Category
Measuring Instruments
Language
English
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