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SmartLab
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115 pages
Manual
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Optics
62
SmartLab:
Automated
Multipurpose
X-ray
Diffractometer
3
Secure it in place with the
Allen wr
ench provided.
4
Connect the
ADPT1,
ADPT2, and
SLIT2 cable to the
ADPT1,
ADPT2,
and SLIT2 connector on
the receiving connector
box.
69
71
Table of Contents
Main Page
Table of Contents
5
Overview
9
Product Features
11
High-Accuracy Theta-Theta Goniometer
11
Attachment
11
X-Ray Generator
11
Cross Beam Optics (CBO)
12
Alignment Mechanism (Monochromators and Analyzers)
12
Receiving Analyzer System
12
Incident Optics System
13
Receiving Optics System
13
Optics Switching System
13
Optical Device Detection
14
Control Software (Smartlab Guidance)
14
Two-Slit SAXS Optics
15
In-Plane Optics (2080B212)
15
Names of Parts
17
Main Unit
17
Goniometer
19
X-Ray Tube
21
Theta_S Arm
22
Theta_D Arm
23
Detector Mounting Bracket
24
Sample Stage and Attachments
24
Software Configuration
25
Control Software
25
Data Processing Software
25
Data Display Software (Options)
25
Analysis Software (Options)
25
Turning on and off Smartlab
27
Turning on Smartlab
27
Starting Smartlab Guidance
27
Startup
28
Shutdown
29
Exiting Smartlab Guidance
30
Turning off Smartlab
30
Opening and Closing the Door
31
Opening the Door
31
Closing the Door
32
Emergency Stop Switch (EMO)
32
Turning On/Off the Internal Lamp (LAMP)
32
Optics
33
CBO Unit (for Cu Target)
33
Incident Optics Unit (Standard Incident Optics Unit)
38
Incident Parallel Slit Adaptor (IPS Adaptor)
38
2-Bounce Monochromator (Option)
41
4-Bounce Monochromator (Option)
44
CBO-F Unit (Option: 2220C301)
46
Incident Slit Box
48
Standard Incident Slit Box
48
Collimator Holder (Option)
50
Receiving Slit Box # 1
54
Standard Receiving Slit Box # 1
54
Receiving Optics Unit # 1
57
Receiving Optical Device Adaptor (ROD Adaptor)
57
2-Bounce Analyzer (Option)
60
Receiving Optics Unit # 2
62
Receiving Parallel Slit Adaptor (RPS Adaptor)
62
Receiving Slit Box # 2
65
Standard Receiving Slit Box # 2
65
Attenuator
67
Standard Attenuator
67
Receiving Optics Unit CALSA (Option: 2680K201)
69
Receiving Parallel Slit
71
CALSA Beam Conditioner
73
Dtector (D/Tex Ultra)
74
Detector
75
Detector Adaptor
75
Scintillation Counter
77
DBM Unit for Cu (Option: 2726H112)
79
D/Tex Ultra (Option: 5741A300)
82
DBM Unit for Cu for D/Tex Ultra (Option: 2726P101)
84
PILATUS (Option: 5742A101)
86
Sample Stage
87
Standard Sample Stage
88
Î’ Sample Stage (Option: 2430B101)
88
Option: 2430H101)
89
For Vertical Transmission Geometry (Option: 2455H105)
90
Antonpaar Sample Stage
92
Attachments
93
Sample Plates
95
Height Reference Sample Plate
95
Transmission SAXS Sample Plate (Option: 2680J111)
95
Capillary Holder (Option: 2430C101)
96
Wafer Sample Plates and Sample Spacers
96
Installing and Removing Sample Spacers
99
Installing and Removing Wafer Sample Plates
100
Sample Holders
101
Glass Sample Holder
101
Aluminum Sample Holder
101
Transmission SAXS Sample Holder (Option: 2680J111)
101
Accessories
103
Examples of Sample Mounting
105
Powder Samples
105
Bulk Samples
105
Sample for Transmission SAXS Measurements
105
Wafer-Shaped Samples
106
Measurements
107
Preparing for Measurements
107
Setting the Hardware Configuration
107
Selecting a Package Measurement
108
Periodic Maintenance
109
Optics Maintenance
109
Cooling Water
110
Cooling Water Filter
110
Target (2080A211/A411)
110
Filament (2080A211/A411)
110
Ion Gauge (Vacuum Gauge) (2080A211/A411)
110
Rotary Pump (2080A211/A411)
110
Troubleshooting
111
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