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8860
Agilent Technologies 8860 Maintaining
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10
Maintaining the TCD
T
o Bakeout Contaminants
from the
TCD
170
Maintain
ing Your GC
169
171
Table of Contents
Default Chapter
3
Table of Contents
3
1 About Maintaining the GC
9
Overview of Maintenance
10
Tools and Materials Required for Maintenance
11
Preparing for Maintenance
13
Viewing Status Data
14
Finding a Replacement Part Number
15
2 Removing Covers
17
To Remove the Detector Top Cover
18
To Remove the Pneumatics Cover
19
To Remove the Electronics Cover
20
3 Maintaining the GC
23
Consumables and Parts for General GC Maintenance
24
Parts Identification
26
To Change the Hydrogen Sensor Calibration Gas Cylinder
27
4 Maintaining Capillary Columns
29
Consumables and Parts for Columns
30
To Install a Capillary Column Hanger
32
To Install Capillary Column Clips
33
To Condition a Capillary Column
34
To Cut a Loop from a Column
37
To Reverse a Column and Bakeout Contaminants
38
5 Maintaining the Split/Splitless Inlet
41
Consumables and Parts for the Split/Splitless Inlet
42
Exploded Parts View of the Split/Splitless Inlet
45
To Install a Capillary Column with the Split/Splitless Inlet
46
To Change the Septum on the Split/Splitless Inlet
50
To Clean the Septum Seat in the Insert Assembly of the Split/Splitless Inlet
52
To Change the Liner and O-Ring on the Split/Splitless Inlet
54
To Replace the Gold Seal on the Split/Splitless Inlet
57
To Replace the Filter in the Split Vent Trap for the Split/Splitless Inlet
59
To Clean the Split/Splitless Inlet
61
To Bakeout Contaminants from the Split/Splitless Inlet
63
6 Maintaining the Purged Packed Inlet
65
Consumables and Parts for the Purged Packed Inlet
66
Exploded Parts View of the Purged Packed Inlet
69
To Install a Capillary Column with the Purged Packed Inlet
70
To Change the Septum on the Purged Packed Inlet
74
To Clean the Septum Seat in the Purged Packed Inlet
76
To Install an Adapter on the Purged Packed Inlet
78
To Change the O-Ring on the Purged Packed Inlet
79
To Change the Glass Liner on the Purged Packed Inlet
80
To Clean the Purged Packed Inlet
82
To Bakeout Contaminants from the Purged Packed Inlet
84
To Install a Packed Metal Column
85
To Install a Packed Column Adapter Onto a Detector
88
To Install a Packed Glass Column
90
To Condition a Packed Column
92
To Install Ferrules on a Packed Metal Column
93
7 Maintaining the Packed Column Inlet
95
Consumables and Parts for the Packed Column Inlet
96
Exploded Parts View of the Packed Column Inlet
98
To Change the Septum on the Packed Column Inlet
99
To Clean the Septum Seat in the Packed Column Inlet
101
To Install an Adapter on the Packed Column Inlet
103
To Change the O-Ring on the Packed Column Inlet
104
To Change the Glass Liner on the Packed Column Inlet
105
To Install an Insulation Cup on the Packed Column Inlet
107
To Clean the Packed Column Inlet
108
To Bakeout Contaminants from the Packed Column Inlet
110
To Install a Packed Metal Column
111
To Install a Packed Column Adapter on a Detector Fitting
113
To Install a Packed Glass Column
115
To Condition a Packed Column
117
To Install Ferrules on a Packed Metal Column
118
8 Maintaining the COC Inlet
119
Consumables and Parts for the Cool On-Column Inlet
120
Exploded Parts View of the Cool On-Column Inlet
123
To Install a Capillary Column with the Cool On-Column Inlet
124
To Check the Needle-To-Column Size on the COC Inlet
127
To Change a Septum on the COC Inlet
128
To Install an Insert on the COC Inlet
130
To Clean the COC Inlet
132
To Replace the 7693A Injector Needle Support Guide
134
To Replace a Needle in a Syringe
135
To Replace the Fused Silica Needle in a Syringe for the COC Inlet
136
To Bakeout Contaminants from the COC Inlet
137
9 Maintaining the FID
139
Consumables and Parts for the FID
140
Exploded Parts Views of the Flame Ionization Detector
142
To Install a Capillary Column in the FID
144
To Replace an FID Jet
147
To Perform Maintenance on the FID Collector Assembly
150
To Check the FID Leakage Current
158
To Check the FID Baseline
159
To Install the Optional FID PTFE Chimney Insert
160
To Bakeout the FID
161
10 Maintaining the TCD
163
Consumables and Parts for the Thermal Conductivity Detector
164
To Install a Capillary Column in the TCD
166
To Bakeout Contaminants from the TCD
169
11 Maintaining the ECD
171
Important Safety Information about the ECD
172
Consumables and Parts for the ECD
174
Exploded Parts View of the Electron Capture Detector
176
To Replace the ECD Fused Silica Indented Mixing Liner and Install the Makeup Gas Adapter
177
To Install a Capillary Column in the ECD
180
To Bakeout the ECD
182
12 Maintaining the NPD
185
Consumables and Parts for the NPD
186
Exploded Parts View of the Nitrogen-Phosphorus Detector
188
To Install a Capillary Column in the NPD
189
To Replace the NPD Bead Assembly
192
To Maintain the NPD Collector, Ceramic Insulators, and Jet
196
To Check the NPD Leakage Current
201
To Bakeout the NPD
202
13 Maintaining the FPD
203
Consumables and Parts for the FPD
204
Exploded Parts View of the Flame Photometric Detector Plus
206
To Install a Capillary Column to the FPD
207
To Change the FPD+ Wavelength Filter
209
To Remove the FPD+ Cover
212
To Replace the FPD+ Ignitor
213
To Install the FPD+ Cover
215
Cleaning the FPD+ Brazement
216
14 Maintaining EPC Modules
217
Consumables and Parts for the Aux EPC
218
Installing or Replacing Frits in the Aux EPC
220
Consumables and Parts for the PCM
222
Calibrating the PCM Interface
223
Installing or Replacing Frits in the PCM
224
15 Maintaining a Valve
227
Consumables and Parts for Valves
228
Exploded Parts View of GC Rotary Valves
229
To Replace a Gas Sampling Valve Loop
230
To Align a Rotary Valve Rotor
232
To Replace a Rotary Valve in the Valve Box
233
To Remove the Upper Valve Box
236
To Install the Upper Valve Box
237
A Swagelok Connections
239
Making Swagelok Connections
240
Using a Swagelok Tee
243
Other manuals for Agilent Technologies 8860
User Manual
86 pages
Installation And First Startup
76 pages
Site Preparation Guide
56 pages
4
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Agilent Technologies 8860 Specifications
General
Brand
Agilent Technologies
Model
8860
Category
Laboratory Equipment
Language
English
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