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Part 2. Packed metal columns Columns and Traps
Procedure: Installing packed metal columns
Procedure: Installing packed metal columns
Before following this procedure, make sure an adapter or liner is installed
(page 128), if needed, and that your column is prepared (page 124.)
Materials required
Prepared metal column
Column adapter, if needed
Wrench
1. Insert the column into the adapter, detector, or inlet liner until it bottoms.
Tighten the nut finger tight.
2. If you are installing a column directly into the detector fitting:
1/4-inch column, tighten an additional 3/4 turn with a 9/16-inch wrench.
1/8-inch column, tighten an additional 1/4 turn with a 7/16-inch wrench.
3. If you are installing a column onto an adapter:
Tighten the column nut using two wrenches in opposition, one on the column
nut and the other on the liner or adapter body. This prevents the liner or
adapter from rotating while you tighten the column nut.
1/4-inch column, tighten an additional 3/4 turn with a 9/16-inch wrench.
1/8-inch column, tighten an additional 1/4 turn with a 7/16-inch wrench.
4. Establish a flow of carrier gas through the inlet. Heat the oven, inlet, and
detector to operating temperatures. Allow them to cool, and then retighten
the fittings.
Adapter
Prepared column