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Fourier 300
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143
Z31980_00_03
T
echnical S
pecifications
2D Experiments
COSYQF
, COSYGPQF
, COSYPH
TOCSYPH, NOESYPH, NOESYGPPH
HSQCGPPH
(1),
HMQCGPQF
(1),
H
MBC-
GPNDQF
(1),
HMBCGPLPN
DQF
(1)
Power Consumption
90 – 230V
ac, 300-400W
T
able 12.8
Software and Environment
142
144
Table of Contents
Main Page
Table of Contents
3
Symbols and Conventions
7
About
7
Policy Statement
7
This Manual
7
Introduction
9
Concept
9
Figure 2.1 the Bruker Fourier 300 System
9
Limitation of Liability
10
Before You Begin
10
Minimum Qualifications for Service Personnel
11
The Bruker Service
11
Transport to Manufacturer
11
Table 2.1 Overview Installation and Operation Requirements for Personnel
11
Safety
13
General
13
Personnel Requirements
13
Qualifications
13
Basic Dangers
14
Unauthorized Persons
14
Personal Protective Equipment
14
General Workplace Dangers
15
Dangers from Electric Power
16
Mechanical Dangers
18
Dangers from Gases under Pressure
19
Dangers from Radiation
20
Dangers Due to High or Low Temperatures
21
Danger from Chemical Substances
22
Environmental Protection
23
Signage
24
Spare Parts
25
Tool Requirements
27
Design and Function
29
Overview
29
Brief Description
29
Figure 5.1 the Fourier 300 Console
29
Figure 5.2 Fourier 300 Console Overview
30
Figure 5.4 Console: Right Side
31
Internal Console Component Layout
31
Figure 5.3 Console: Left Side
31
Figure 5.5 Console: Front View
32
Figure 5.6 Location of the Console Air Filter Tray
32
Unit Descriptions
33
Intelligent Devices with Ethernet
33
Figure 5.7 Console Input and Output Connections
33
Main Board
34
Figure 5.8 DDS2
34
Figure 5.9 DDS1
34
Intelligent Devices with Can-Bus
35
Lock System
35
Variable Temperature Unit (VTU)
35
Shim Control
36
Figure 5.10 Two Shim Boards
36
Peripheral Control Board
37
GAB/2 Backplane
37
Intelligent Devices with LVDS
37
Devices Without Interface
37
Table 5.1 Preamplifiers
38
Preamplifiers
38
Lock Switch
38
Transmitters
38
Figure 5.11 Lock Switch
39
Figure 5.12 Lock Switch Block Diagramm
39
Power Supplies
40
Figure 5.13 Lock Switch Connections & LEDS
40
Ventilators
41
Figure 5.14 Ventilator
41
Connections
42
Figure 5.15 Connections
42
Accessories
43
Installation
45
Unpacking
45
Wiring up
45
Adjusting Air Pressure
46
Switch on for the First Time
46
Checking that the Console Has Booted
46
Figure 6.1 Checking the DHCP Server
47
Performing Cf on a Fourier
48
Setting the Spectrometer Frequency
49
Editing the Nuclei List
50
Cortab and Power Check
50
ETH Addresses and Tty Settings
50
RF Routing
52
Additional Configurations
53
Installation of Pulse Programs and Parameter Sets
54
Editing Solvents
56
Configuring the Probe
57
Configuring the Lock Parameters
59
Configuring the Transmitter and Preamplifier Pre-Delays
61
Working with the Lock System
62
The Lock System
62
Setting the Magnet to the Right Field
62
Finding a Lock
63
Figure 6.2 Result of Flock with One Solvent Peak
67
Converting the Parameter Set to the Actual BF1
70
Tuning and Matching the Probe
71
General Information about the Fourier Probe
71
The Gradshim Command
71
Figure 6.3 Gradient Echo
72
Installation Acceptance
74
Table 6.1 Hard Specs for the Fourier
75
Main Differences between Fourier & Avance Systems
76
Configuration
77
Network Settings
77
Figure 7.1 Fixed User Specific IP Address
77
Figure 7.2 Power up Jumper
78
Resetting the CPU
79
Firmware Update
79
Ethernet Devices (Main Board, Lock Board, VTU)
79
4.3.2 CAN-Bus Devices
80
Lock Control and VTU
83
FPGA Update
83
Main Board
84
Device Specific Settings & Tools
85
Main Board
86
BIS EEPROM Settings
86
Board Temperature Control
88
On-Board Voltages
90
4.5.1.5 Pulse Programmer Memory
90
Shim Control
91
GAB/2 Interface
95
Lock Board
96
Vtu
105
Changing PID Parameters
106
Setting the Heater Protection Threshold
107
Calibrating the Thermocouple
108
Peripheral Control
108
Setting the Lift Parameters
109
Setting the Spin Parameters
109
Setting the Spin Safety Threshold
110
Calibrating and Measuring the Helium Level
111
Monitoring the Console and Shim Stack Temperature
113
Additional Test Applications
114
Pulse Programming
119
General Principle
119
Structure of Pulse Programs
119
Syntax and Examples
120
Table 8.1 Structure of Pulse Programs
120
Wiring Schedules
127
10 Maintenance and Repairs
135
Figure 10.1 the Filter Tray
135
Safety
137
Cleaning
137
Disposal
137
11 Cleaning and Disposal
137
Dismantling
138
Disposal Intructions
138
12 Technical Specifications
141
Table 12.1 Transmit Channels
141
Table 12.2 Receiver Channel
141
Table 12.3 Gradient Control
141
Table 12.4 Shim System
141
Table 12.8 Software and Environment
142
Table 12.5 Lock System
142
Table 12.7 N2 Temperature Controller
142
Table 12.6 Peripheral Control
142
13 Contact
145
Appendix
147
Warning Signs
147
Figures
149
Tables
151
Index
153
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