74
Z31980_00_03
Installation
i
IMPORTANT: To start gradshimming using the "shim" button of the flow bar and also
from IconNMR, it is necessary to store the current configuration for automation. (Setup -
> store for automation). The flow bar or ICON will call either a 1H or a 2H gradshim,
depending on what was selected when the setup was stored for automation.
For further information on gradshim please check the respective manual.
i
Note: Gradshim uses differnt parameters on a Fourier. Be sure to define the parameter
sets gradshim1d1h_f or gradshim1d2h_f when creating a shim map.
6.13 Installation Acceptance
i
Note: All the for the Fourier 300 necessary Hardware Tests (HWT) were carried out dur-
ing console end testing and are not intendend to be repeated at the customer site.
The following ATP tests are carried out on the FOURIER during customer acceptance
• Determination 90 degree 2H observe pulse
• Determination 90 degree 1H observe pulse
• Determination 90 degree 13C observe pulse
• Determination 90 degree 1H decoupling (CPD) pulse
• Determination 90 degree 1H high power decoupling pulse
• Determination 90 degree 13C low power decoupling pulse
• Lineshape test for 1H with rotation
• Resolution test for 1H
• Sensitivity test for 1H
• Lineshape Test for 13C with rotation
• Resolution test for 13C
• Sensitivity test for 13C (ASTM)
• Sensitivity test for 13C (EB)
• HSQC experiment with Z-gradient (console test)
• COSY experiment with Z-gradient (console test)
• DEPT-90 experiment
• DEPT-135 experiment