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Bruker Fourier 300 - Installation Acceptance Tests

Bruker Fourier 300
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74
Z31980_00_03
Installation
i
IMPORTANT: To start gradshimming using the "shim" button of the flow bar and also
from IconNMR, it is necessary to store the current configuration for automation. (Setup -
> store for automation). The flow bar or ICON will call either a 1H or a 2H gradshim,
depending on what was selected when the setup was stored for automation.
For further information on gradshim please check the respective manual.
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Note: Gradshim uses differnt parameters on a Fourier. Be sure to define the parameter
sets gradshim1d1h_f or gradshim1d2h_f when creating a shim map.
6.13 Installation Acceptance
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Note: All the for the Fourier 300 necessary Hardware Tests (HWT) were carried out dur-
ing console end testing and are not intendend to be repeated at the customer site.
The following ATP tests are carried out on the FOURIER during customer acceptance
Determination 90 degree 2H observe pulse
Determination 90 degree 1H observe pulse
Determination 90 degree 13C observe pulse
Determination 90 degree 1H decoupling (CPD) pulse
Determination 90 degree 1H high power decoupling pulse
Determination 90 degree 13C low power decoupling pulse
Lineshape test for 1H with rotation
Resolution test for 1H
Sensitivity test for 1H
Lineshape Test for 13C with rotation
Resolution test for 13C
Sensitivity test for 13C (ASTM)
Sensitivity test for 13C (EB)
HSQC experiment with Z-gradient (console test)
COSY experiment with Z-gradient (console test)
DEPT-90 experiment
DEPT-135 experiment

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