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Shimadzu GC-2014 Operation Manual

Shimadzu GC-2014
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4.10 Flow controller (SPL, WBI only)
100
Trap replacement
Replace traps by the following procedures.
(1)
Stop carrier gas supply.
(2)
Remove INJ/DET cover.
(3)
To avoid error, replace the traps one by one.
(4)
Remove the blind from a new trap.
This blind has been used for sealing the inside of
the trap. You don't need the blind any more.
(5)
Install the new trap.
The tubing codes are as follows.
S ............ Split flow line
P ............ Septum purge flow line
C ............ Carrier gas inlet flow line
DO NOT forget to insert a couple of aluminum
gaskets between G-type joints.
Conditioning molecular sieve filter
To condition molecular sieve filter, use the following procedures.
(1)
Stop carrier gas supply.
(2)
Remove INJ/DET cover.
(3)
Remove molecular sieve filter.
(4)
Condition the filter to the following conditions.
Flow direction of N
2
or He gas
Opposite direction of the GC normal operation
Gas flow rate...........10 to 20 ml/min
Temperature............300C
Time ........................3 to 4 hours
(5)
After conditioning, immediately reinstall the
molecular sieve filter so that the filter does not get
contaminated.
G-type joint connection
GM joint
Column aluminum
gaskets (2 to 3 pcs)
GF joint

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Shimadzu GC-2014 Specifications

General IconGeneral
TypeGas Chromatograph
DisplayLCD
Maximum Heating Rate120°C/min
Data AcquisitionDigital
Maximum Number of Detectors4
WeightApprox. 45 kg
Carrier GasHelium, Nitrogen, Hydrogen
Detector OptionsFID, TCD, ECD, FPD
Injection PortSplit/Splitless, On-column
Gas ControlElectronic Flow Control (EFC)
Temperature Programming Rate0.1 to 120 °C/min
Power Requirements230 V AC, 50/60 Hz
Detector Temperature RangeUp to 400°C (depending on detector type)

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