Shimadzu GC-2014 Operation Manual

59
3.3 Analysis using capillary column
3
 Installing capillary column in oven
1
Attach graphite ferrule to injection port end of
column.
(1) After slipping a box nut over the injection port end
of capillary column, slip the graphite ferrule.
(2) Using the ferrule adjuster, fix the graphite ferrule
temporarily.
(3) Let the end of capillary column stick out approx.
10 mm from the ferrule adjuster, cut the column at
the end of ferrule adjuster by using capillary
cutter, etc.
By using ferrule adjuster for SPL, you can fix the
ferrule at 34 mm from the column end.
Ferrule adjuster
Graphite ferrule
Box nut
Capillary cutter
NOTE
When performing splitless analysis by using the wide
bore column with 0.53 mm of inside diameter, fix the
graphite at 15 mm from column end.

Shimadzu GC-2014 Specifications

General

Type	Gas Chromatograph
Display	LCD
Maximum Heating Rate	120°C/min
Data Acquisition	Digital
Maximum Number of Detectors	4
Weight	Approx. 45 kg
Carrier Gas	Helium, Nitrogen, Hydrogen
Detector Options	FID, TCD, ECD, FPD
Injection Port	Split/Splitless, On-column
Gas Control	Electronic Flow Control (EFC)
Temperature Programming Rate	0.1 to 120 °C/min
Power Requirements	230 V AC, 50/60 Hz
Detector Temperature Range	Up to 400°C (depending on detector type)