Shimadzu GC-2014 Operation Manual

63
3.3 Analysis using capillary column
3
 Checking gas leak
• After installation of column, etc., has been completed, perform a leak check. If there is leakage in the flow line,
you will not obtain high reproducibility in your analysis, and also can waste carrier gas.
• Specify temperature, etc., temporarily when checking.
1
Prepare carrier gas.
2
Turn on the power.
3
Press .
Specify "Start time" to the required time for the leak
check.
Verify that "Yes" is selected on "Start Temp/Det".
OFF ON

Shimadzu GC-2014 Specifications

General

Type	Gas Chromatograph
Display	LCD
Maximum Heating Rate	120°C/min
Data Acquisition	Digital
Maximum Number of Detectors	4
Weight	Approx. 45 kg
Carrier Gas	Helium, Nitrogen, Hydrogen
Detector Options	FID, TCD, ECD, FPD
Injection Port	Split/Splitless, On-column
Gas Control	Electronic Flow Control (EFC)
Temperature Programming Rate	0.1 to 120 °C/min
Power Requirements	230 V AC, 50/60 Hz
Detector Temperature Range	Up to 400°C (depending on detector type)