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Shimadzu GC-2014 Operation Manual

Shimadzu GC-2014
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41
3.2 Analysis using packed column
3
Setting for analysis
1
Specify the dual AFC setting.
(1) Press .
(2) Select "Dual" on "Control mode".
(3) Specify the flow rate of left and right of AFC
respectively.
2
Specify the detectors.
(1) Press .
(2) Select "Dual" on "Control mode".
(3) Specify "Signal polarity" according to the position
of the FID to be used in analysis (left: +, right: ).
(4) Specify the temperature.
NOTE
In the description of this section, you specify the injection port as dual packed INJ mode, and the detector as dual FID
mode. If you use the GC as single INJ/single FID, change the corresponding part of the setting.
If the computer is connected, specify the following on the computer.
CAUTION
If you have connected columns to both flow lines of
the dual packed INJ, ALWAYS select "Dual" and
specify the flow rate of both lines. If "Single" is
selected, since carrier gas flows only in one column,
it may deteriorate the other column when you raise
the oven temperature.

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Shimadzu GC-2014 Specifications

General IconGeneral
TypeGas Chromatograph
DisplayLCD
Maximum Heating Rate120°C/min
Data AcquisitionDigital
Maximum Number of Detectors4
WeightApprox. 45 kg
Carrier GasHelium, Nitrogen, Hydrogen
Detector OptionsFID, TCD, ECD, FPD
Injection PortSplit/Splitless, On-column
Gas ControlElectronic Flow Control (EFC)
Temperature Programming Rate0.1 to 120 °C/min
Power Requirements230 V AC, 50/60 Hz
Detector Temperature RangeUp to 400°C (depending on detector type)

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