Shimadzu GC-2014 Operation Manual

3.3 Analysis using capillary column
60
2
Attach graphite ferrule to detector end of
column.
(1) Using the ferrule adjuster for FID, fix the graphite
ferrule in the same procedure as in the case of
the injector port end.
You can fix the ferrule at 99 mm from the column
end.
(2) Adjust the ferrule position (L).
FID:Refer to " Length from column end to ferrule"
P. 6 1
TCD:89 mm
Injection port end Detector end
Ferrule
Box nut
Column
nut (with
split)
L
34 mm
Ferrule
adjuster
Ferrule
*The graphite ferrule is fixed, using
the ferrule adjuster.
FID: L=99 mm
(Refer to " Length from column end
to ferrule" P.61)
TCD: L=89 mm
NOTE
• For the detector end, you will use Column nut (with
split). You don't need to place the nut before graphite
ferrule.
• You can insert some narrow columns into the
standard FID jet. But in these cases, the detector
gases may not flow correctly. We recommend you to
adjust L=95-96 mm. for the standard FID jet.
Refer to " Length from column end to ferrule" P.61 for the
type of FID jet types.

Shimadzu GC-2014 Specifications

General

Type	Gas Chromatograph
Display	LCD
Maximum Heating Rate	120°C/min
Data Acquisition	Digital
Maximum Number of Detectors	4
Weight	Approx. 45 kg
Carrier Gas	Helium, Nitrogen, Hydrogen
Detector Options	FID, TCD, ECD, FPD
Injection Port	Split/Splitless, On-column
Gas Control	Electronic Flow Control (EFC)
Temperature Programming Rate	0.1 to 120 °C/min
Power Requirements	230 V AC, 50/60 Hz
Detector Temperature Range	Up to 400°C (depending on detector type)