Agilent Technologies 7890B - Page 87

Chromatographic Checkout 6
Operation Manual 87
Initial time 0 min
Rate 1 10 °C/min
Final temp 105 °C
Final time 0 min
Rate 2 20 °C/min
Final temp 2 190 °C
Final time 2 7.25 min for sulfur
12.25 min for phosphorus
ALS settings (if installed)
Sample washes 2
Sample pumps 6
Sample wash volume 8
Injection volume 1 µL
Syringe size 10 µL
Solvent A pre washes 2
Solvent A post washes 2
Solvent A wash volume 8
Solvent B pre washes 0
Solvent B post washes 0
Solvent B wash volume 0
Injection mode (7693A) Normal
Airgap Volume (7693A) 0.20
Viscosity delay 0
Inject Dispense Speed (7693A) 6000
Plunger speed (7683) Fast, for all inlets except COC.
PreInjection dwell 0
PostInjection dwell 0
Manual injection
Injection volume 1 µL
Data System
Data rate 5 Hz
Table 9 FPD
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Phosphorus Checkout Conditions (continued)