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Bruker HYPERION User Manual
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165
Bruker Optik GmbH
HYPERION User Manual
Specifications A
A.7
Heatable sample holder
Parameter
S
pecification
max. tem
perature
180
°
C
T
emperature variations
1
°
C at 150°C
max. diamete
r of the sample positi
on
13 mm
Dimension of the heat
able sample holder
75 mm x 50 mm x 10 mm
Dimension of the temperature
controller
260 mm x 150 mm x 270 mm
Cable length
~ 50 cm
Power supply re
quirement
s
230V
, 100W
, 50/60Hz
166
168
Table of Contents
Default Chapter
3
Table of Contents
3
1 Safety
7
General Safety Information
7
Classification of the Safety Notes
7
Overview of Possible Types of Hazard
8
Possible Hazards During Installation, Operation, Maintenance and Repair
8
Possible Hazardous Sample Materials
9
Intended Use
10
Service Contact Data
10
2 Installation
11
General Information
11
Inspecting the Packaging
11
Transporting the Microscope
11
Scope of Delivery
12
Site Requirements
13
Connecting the Microscope to the Power Supply
15
General Information
15
Safety Note
15
Procedure
16
Cable Connections
17
Overview of the Connection Sockets
17
Connecting the Motorized Microscope Stage
19
Connecting the Joystick
20
Connecting the Video Camera
20
Connecting the MCT Detector(S)
21
Connecting the FPA Detector
22
Connecting the Microscope to the Spectrometer
24
Connecting the Microscope to the Purge Gas Supply Line
25
General Information
25
Procedure
25
3 Overview
27
Microscope Variants
27
Complete Overview - Operating Elements & Components
28
Operating Panel
31
Brightness Control and Brightness Indicator
32
Microscope Stages
33
Overview 3
33
Manual Stage
34
Focus Control Elements
35
Motorized Stage
36
Joystick-Controlled Stage Movement
37
Condenser
38
Apertures
39
Overview
39
Installation Locations of the Apertures
41
Manual Knife-Edge Aperture
42
Iris Aperture for Setting the Koehler Illumination
43
Light Path Selector Lever
44
Revolving Nosepiece and Objectives
45
Binocular
47
LCD Monitor
48
Detectors
49
Installation Locations
49
Types of Detector
50
Beam Path
51
Possible Instrumental Setups
55
4 Operation
57
General Information
57
Switching on / off the Analysis System
58
Preparing the Microscope for a Spectroscopic Measurement
60
Cooling the Detector
61
General Information
61
Safety Notes
61
Funneling Liquid Nitrogen in the Detector
62
Resetting the Motorized Stage
64
Checking and Correcting the Condenser Setting
65
Checking the IR Signal Intensity
68
Procedure in Transmission Mode
68
Procedure in Reflection Mode
70
Procedure with ATR Objective
74
Checking the Detector Saturation
77
Viewing the Sample and Selecting the Measurement Area
79
Viewing and Measuring a Sample in Transmission
80
Viewing and Measuring a Sample in Reflection
84
ATR Objective - Important Operating Notes
88
General Handling Instructions
88
Cleaning the ATR Crystal
88
Attaching the ATR Objective at the Revolving Nosepiece
89
Setting the Viewing Mode / Measuring Mode at the ATR Objective
90
Setting Contact Pressure Levels
91
Focussing
91
Measuring a Sample with the ATR Objective (Single Point Measurement)
93
Measuring a Sample with the ATR Objective (Mapping Measurement)
97
GIR Objective - Important Operating Notes
101
General Information
101
Design of the Mirror Optics
102
Setting the Viewing Mode (VIS) or Measuring Mode (GIR)
103
Images Generated by the GIR Objective
104
Checking the Alignment of the GIR Objective
105
Realigning the GIR Objective
106
Measuring a Sample with the GIR Objective
109
Purging the Microscope
112
5 Options and Accessories
113
Optional Objectives
113
Overview
113
Additional Information about the GIR Objective
114
Optional Apertures
115
Overview
115
Installation Location of the Exchangeable Apertures
116
Optional Microscope Stages and Sample Holders
118
Overview
118
Heating/Freezing Stage THMS 600 (Linkam)
119
General Information
119
Controlling the Temperature
119
Safety Notes
120
Heatable Sample Holder
120
General Information
120
Safety Notes
121
Controlling the Temperature
121
Polarizer
122
General Information
122
Safety Notes
122
Installation Location
123
Performing IR Spectroscopic Analyses Using Polarized Light
124
External Sample Cabinet - IMAC
125
Compression Cells
126
6 Repair and Maintenance
127
General Information
127
Removing and Installing the Detector
127
Removal and Installation Procedure of the MCT Detector
127
Removal and Installation Procedure of the FPA Detector
130
Evacuating the Detector Dewar
132
General Information
132
Evacuating the MCT Detector Dewar
132
Replacing a Damaged ATR Objective Crystal
137
General Handling Instructions
137
Checking the ATR Crystal for Damages
137
Replacing the ATR Crystal Assembly
138
Checking the ATR Crystal Position for Centrality
143
Aligning the ATR Crystal Centrically
144
Checking the Height Setting of the ATR Crystal
145
Correcting the Height Setting of the ATR Crystal
146
7 Troubleshooting
149
General Information
149
Problem - Possible Cause - Solution
150
Sample Viewing through the Binocular: no Field of View or Dark Field of View
150
No Video Image Is Displayed on the LCD Monitor And/Or in OPUS
151
No IR Signal Is Detected or the Detected IR Signal Intensity Is too Low
152
IR Signal Check in OPUS Shows an Unusual Spectrum Curve Shape
155
Problems Regarding the Motorized Microscope Stage
156
Problems Regarding the ATR Objective
157
Problems Regarding Mapping Measurements
159
Problems Regarding the FPA Detector
160
Specifications
163
HYPERION Microscope
163
Objectives
163
Motorized Microscope Stage
164
Manual Microscope Stage
164
Detectors
165
A.5 Detectors
165
Heating / Freezing Sample Stage THMS600 (Linkam)
166
Heatable Sample Holder
167
B Measurement Parameters
169
C Spare Parts and Consumables
173
D System Diagram
175
4
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Bruker HYPERION Specifications
General
Brand
Bruker
Model
HYPERION
Category
Microscope
Language
English
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