Shimadzu GCMS-QP2010 Series - Page 60

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4 Qualitative Analysis

46 GCMS-QP2010 Series Operation Guide

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Table of Contents11
Overall Configuration of Gcmssolution15
Programs15
Flowchart of Operating Procedure16
Starting GC/MS17
Turning on the Power17
Layout of Operating Areas18
Inspecting Consumable Items and Maintenance Parts19
System Configuration20
Setting the Modules Used for Analysis20
Checking Column Information21
Enabling the Modules Used for Analysis23
Vacuum System Startup24
Checking for Vacuum Leakage25
Autotuning27
Setting Analysis Conditions27
Executing Autotuning28
Checking Autotuning Results31
Creating a Folder32
Creating a Folder with Data Explorer32
Qualitative Analysis34
Creating a Method File34
Setting Autosampler Parameters35
Setting GC Parameters35
Setting MS Parameters36
Setting Similarity Search Parameters37
Saving the Method File39
Repeating Autotuning39
Sequential Analysis40
Creating a Batch File40
Editing a Batch File ^ Ver. 2.543
Saving Batch Files46
Executing Sequential Analysis47
Analyzing Data48
Loading Data Files48
Zoom in on a Peak in the Chromatogram and Displaying Mass Spectra49
Removing the Background51
Searching for Similarity ^ Ver. 2.552
Displaying Mass Chromatograms53
Registering Spectra Displayed for Target Compounds ^ Ver. 2.554
Editing the Spectrum Process Table54
Saving Data Files56
Printing Qualitative Analysis Reports57
Loading Report Formats57
Editing Report Formats58
Outputting Reports61
Quantitative Analysis62
Creating a Method File62
Creating a Compound Table62
Creating a SIM Table67
Sequential Analysis69
Creating a Batch File69
Editing a Batch File ^ Ver. 2.572
Saving Batch Files72
Executing Sequential Analysis73
Analyzing Data74
Checking and Correcting Calibration Curves74
Re-Quantifying after Correcting a Calibration Curve81
Checking and Correcting Quantitation Results83
Printing Quantitative Analysis Reports87
Creating and Outputting Quantitative Analysis Reports87
Shutting down GC/MS90
Vacuum System Shutdown90
Turning off the Power91
File Format92
Appendix B Viewing Help93
Viewing Help93
Displaying Help from the Assistant Bar93
Displaying Help from the Menu Bar93
Displaying Help with the F1 Key94
Appendix C Using Data Explorer95
Appendix D Maintenance97
Maintenance97
Easy Stop99
(Applicable to QP2010 Ultra and QP2010 SE Models)99
Reset Procedure for Usage Frequencies and Usage Times ^ Ver.2.5101
Changing Replacement Guidelines for Septa and Glass Inserts103
Single Analysis (Manual Injection)106
Appendix F Index Searches108
Appendix G Displaying Chromatograms110
Displaying Chromatograms from Fragment Tables110
Displaying Chromatograms from Mass Spectra112
Editing Batch Files113
Adding Batch Files (Batch Queue)115
Creating Batch Files to Add115
Adding Batch Files116
Appendix I Reducing the Carrier Gas Flow Rate after Sequential119
Reducing the Carrier Gas Flow Rate after Sequential Analysis119
Creating a Method File that Reduces the Carrier Gas Flow Rate119
Creating Batch Files120
Ecology Mode123
(This Feature Applies to QP2010 Ultra and QP2010 SE Models.)123
Setting the Mode Manually123
Setting the Mode Using Batch Processing124
Printing Reports126
Printing Images126
(Printing Spectra and Chromatograms Displayed in Windows)126
Creating Reports128
Using Templates128
Using Previously Created Report Files129
Manually Setting Report Content130

Shimadzu GCMS-QP2010 Series - Page 60

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