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Running Multiple-Vial Analyses
Recalibrating With the Same Group of Standards
• each sample is analyzed once,
• the calibration standards are analyzed twice before the samples and re-analyzed
twice after every 5 samples,
C1 C2 C3 S10-S14 C1 C2 C3 S15-S19 C1 C2 C3 S20-S24 C1 C2 C3
• the calibration standards are located in positions 90 to 92 of the autosampler tray,
• the 15 sample vials are located in positions 10 to 24 of the autosampler tray, and
• the samples and standard are analyzed using a method called METH1.
The example assumes that the sequence table is empty. If the sequence table is not
empty, use the All Lines item, accessed by pressing the Delete button [F6].
1 Select the Sequence button [F4] in the Analysis screen.
2 For sequence line 1, select the Insert button [F7] and enter:
Vial Range 10 to 24
#Inj 2
Inj. Volume Default
Method METH1
3 Select the Calibration button [F1] to display the Calibration Settings screen for
sequence line 1 and choose Edit.
4 Enter the following information:
Calibration vial
range 90 to 92
Number of
injections 2
Calibration
method METH1
Recalibrate every 5 vials multi
Before On
After Off
5 Select the Done button [F6] to accept entries.
6 Select the Start button [F8] in the Sequence screen.
7 Press the Enter key start the sequence.
c
The autosampler now analyzes:
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