58 Operation Manual
6 Chromatographic Checkout
• Check that the flame is lit.
• Check that the signal is set to the correct detector.
7 Create or load a method with the parameter values listed
in Table 4.
Table 4 FID Checkout Conditions
Column and sample
Type HP-5, 30 m × 0.32 mm × 0.25 µm
(19091J-413)
Sample FID checkout 5188-5372
Column flow 6.5 mL/min
Column mode Constant flow
Split/splitless inlet
Temperature 250 °C
Mode Splitless
Purge flow 40 mL/min
Purge time 0.5 min
Septum purge 3 mL/min
Gas saver Off
Multimode inlet
Mode Splitless
Inlet temperature 75 °C
Initial time 0.1 min
Rate 1 720 °C/min
Final temp 1 250 °C
Final time 1 5.0 min
Purge time 1.0 min
Purge flow 40 mL/min
Septum purge 3 mL/min
Packed column inlet
Temperature 250 °C
Septum purge 3 mL/min
Cool on-column inlet
Temperature Oven Track
To Next Page
Loading...
Need help?
General
