Thermo Scientific TSQ Altis, Quantis, and Fortis Hardware Manual xiii
Figure 1. Block diagram of MS hardware components . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5
Figure 2. Ion optics and mass analyzer assemblies . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
Figure 3. Placement of the turbomolecular pump next to the vacuum manifold . . . . . . . . 10
Figure 4. Functional block diagram of the Altis vacuum system . . . . . . . . . . . . . . . . . . . . 12
Figure 5. Gas inlets and vacuum (foreline) port (left side of the MS) . . . . . . . . . . . . . . . . 16
Figure 6. API source interface for the TSQ Altis MS (cross section) . . . . . . . . . . . . . . . . . 18
Figure 7. Altis ion transfer tube . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19
Figure 8. Quantis ion transfer tube . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19
Figure 9. Fortis ion transfer tube . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19
Figure 10. Altis RF Lens and exit lens . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20
Figure 11. Quantis RF lens . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20
Figure 12. Fortis exit lens . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21
Figure 13. MP00 lens (left) and lens L0 (right) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 23
Figure 14. MP0 multipole with neutral beam blocker (1) . . . . . . . . . . . . . . . . . . . . . . . . . . 24
Figure 15. EL11 (left) and EL12 (right) lenses . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 24
Figure 16. LEDs on the instrument front panel . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 25
Figure 17. Power entry module . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 26
Figure 18. Communication connectors (right side of the MS) . . . . . . . . . . . . . . . . . . . . . . 28
Figure 19. Main power switch on the power module . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 32
Figure 20. Electronic service switch and main power switch . . . . . . . . . . . . . . . . . . . . . . . 34
Figure 21. Reset button (1) on the communication panel . . . . . . . . . . . . . . . . . . . . . . . . . . 36
Figure 22. Electronic service switch and main power switch . . . . . . . . . . . . . . . . . . . . . . . 37
Figure 23. Connection to the H-ESI or the low-flow H-ESI source. . . . . . . . . . . . . . . . . . 52
Figure 24. Connection to the APCI spray insert . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 53
Figure 25. Syringe pump settings box . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 57
Figure 26. Define Scan parameters . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 58
Figure 27. Plot Chromatogram dialog box . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 59
Figure 28. Calibration pane options. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 61
Figure 29. Report Generation Options . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 61
Figure 30. Error range for the EMRS calibrants . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 62
Figure 31. Ion signal intensity as a function of the lens L0 offset voltage . . . . . . . . . . . . . . 63
Figure 32. Mass spectrum of EMRS in positive ion mode . . . . . . . . . . . . . . . . . . . . . . . . . . 64
Figure 33. Mass spectrum of EMRS in negative ion mode . . . . . . . . . . . . . . . . . . . . . . . . . 65
Figure 34. Optimizing the source parameters in the Optimization pane . . . . . . . . . . . . . . 69
Figure 35. Example optimization of the RF lens (SRIG RF) tuning for m/z 997.55 . . . . . . 70
Figure 36. Examples of the optimization results tables . . . . . . . . . . . . . . . . . . . . . . . . . . . . 70
Figure 37. Illustration of product scan type . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 74
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