xviii Table of Contents
Chapter 3
Preparing Your 600E System for Operation
.................................................. 27
3.1 Sparging Eluents.............................................................................................. 28
3.2 Priming the Pump............................................................................................ 31
3.3 Daily Routine Operation ................................................................................. 34
3.4 Flushing the System ........................................................................................ 35
3.4.1 Flushing the System Fluid Lines ...................................................... 36
3.4.2 Flushing the Rheodyne Manual Injector ........................................... 36
3.4.3 Purging the Autoinjector ................................................................... 37
3.4.4 Reconnecting the Column After Flushing the System ...................... 37
3.5 Equilibrating the System ................................................................................. 38
3.6 Changing Eluents ............................................................................................ 41
3.6.1 Adding Fresh Eluent ......................................................................... 41
3.6.2 Changing Between Incompatible Eluents ......................................... 42
Chapter 4
Setting PowerLine Controller Operating Parameters
............................... 45
4.1 Setting Up the 600 as a PowerLine Controller................................................ 47
4.1.1 Configuring the Controller Type ....................................................... 49
4.1.2 Selecting an Integrator ...................................................................... 51
4.1.3 Selecting the Report Type ................................................................. 54
4.2 Verifying that PowerLine Devices Are Active................................................ 61
4.3 Setting Up the 600E Pump.............................................................................. 63
4.3.1 Accessing the Pump Setup Screen .................................................... 65
4.3.2 Setting Pump Setup Parameters ........................................................ 66
4.3.3 Exiting the Pump Setup Screen ........................................................ 71
4.4 Setting Up the Autoinjector............................................................................. 71
4.4.1 Accessing the Autoinjector Setup Screen ......................................... 73
4.4.2 Setting Autoinjector Setup Parameters ............................................. 74
4.4.3 Exiting the Autoinjector Setup Screen .............................................. 75