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Agilent Technologies 6500 Series - To Clean the Capillary

Agilent Technologies 6500 Series
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Agilent 6500 Series Q-TOF LC/MS Maintenance Guide 115
Maintenance 2
To clean the capillary
To clean the capillary
When required When you observe decreased sensitivity and decreased signal stability
Tools required 5190-1401 Cleaning Powder, Dielectric Capillary
100mL polypropylene graduated cylinder, or glass-graduated cylinder with
two 1 mL pipette tip
Parts required Powdered Precision Cleaner (Alconox catalog number 1104)
1 Dissolve 1 g Alconox Powdered Precision Cleaner in 100 mL deionized
water.
This concentration is the recommended concentration for “manual or
ultrasonic cleaning”.
2 Place the ion transport capillary upright in a 100 mL polypropylene
graduated cylinder and fill with Alconox solution.
3 Sonicate the graduated cylinder with the ion transport capillary in an
ultrasonic cleaner for 10 to 15 minutes.
You may use a 1 mL pipette over the end of the ion transport capillary to
protect the metallized plating. Trim the pipette tip to approximately 4 cm so
that the capillary can be immersed in the cleaning solution.

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