Agilent Technologies 6890 Series Service Manual

610 Checkout Chromatograms
FID checkout conditions and chromatogram
2 of 26
Jun 2001
Performance Verification
Agilent 6890 Gas Chromatograph Service Manual
FID checkout conditions and chromatogram
Column and sample
Type HP-5 30 m × 0.32 mm × 0.25 µm PN 19091J-413
Sample FID Checkout PN 18710-60170
Injection volume 1 µL
Inlet
Temperature 250°C Purged/Packed or Split/Splitless
Oven Track Cool On-Column
Inlet pressure 25 psi (Constant pressure for EPC inlets,
helium)
Split/Splitless Only
Mode Splitless
Purge flow 60 mL/min
Purge time 0.75 min
PTV—Splitless Mode
Inlet temperature 40°C
Initial time 0.1 min
Rate 1 720°C/min
Final temp 1 350°C
Final time 1 2 min
Rate 2 100°C/min
Final temp 2 250°C
Final time 2 0 min
Inlet pressure 25 psi (const. press. for EPC inlets)
Mode Splitless
Purge time 0.75 min
Purge flow 60 mL/min
Detector
Temperature 300°C
H
2
flow 30 mL/min
Air flow 400 mL/min
Makeup flow, N
2
25 mL/min
Offset Should be < 20 pA

Agilent Technologies 6890 Series Specifications

General

Brand	Agilent Technologies
Model	6890 Series
Category	Laboratory Equipment
Language	English