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Jun 2001
Detectors
Agilent 6890 Gas Chromatograph Service Manual
Thermal Conductivity Detector (TCD) 330
Cleaning the Thermal Conductivity Detector
Cleaning the Thermal Conductivity Detector
After verifying that the carrier supply gas and flow system components are
leak- and contaminant-free, you can clean the detector by bakeout.
1. Turn off the detector.
2. Remove the column from the detector, then cap the detector column
fitting.
3. Establish a normal reference gas flow rate (20 to 30 mL/min) through
the detector (set oven temperature to 250°C).
4. Heat the detector to 400°C. Allow thermal cleaning to continue for several
hours.