CEM liberty - Run History Reports; Creating a Run History Report; Sample Run History Report

Liberty
™
Automated Microwave Peptide Synthesizer
600178 • Revision 5 • October 2009
56
Run History Reports
Run History Reports record each command executed by PepDriver during a run with a date/time
stamp. In addition, a Run History Report records any system errors that occur, allowing for easy
diagnosis and troubleshooting of failed syntheses.
Creating a Run History Report
From the Run History tab:
Open the folder for the month in which the method was run.1.
Right-click on the specic run to be reported and select Display Run History 2.
Detail.
The Report Viewer window will open, and the method report will be rendered as 3.
a PDF.
Click Save As PDF to save the report.4.
Sample Run History Report
Run History
Action
Time
ACP
7/17/2009 9:35:06 AM
Pressurize - ALL
7/17/2009 9:35:09 AM
Pressurize DMF
7/17/2009 9:35:09 AM
Pressurize DCM
7/17/2009 9:35:12 AM
Pressurize Deprotect
7/17/2009 9:35:16 AM
End Pressurize
7/17/2009 9:35:21 AM
Starting Method
7/17/2009 9:35:21 AM
Initialization and Resin Loading
7/17/2009 9:35:21 AM
Clean Reaction Vessel - Unfiltered
7/17/2009 9:35:52 AM
DMF_Bottom (7.0/6.1)
7/17/2009 9:36:20 AM
Add DMF to Resin
7/17/2009 9:37:58 AM
Depressurize N2
7/17/2009 9:38:40 AM
Purge All to Resin
7/17/2009 9:38:46 AM
Add DCM to Resin
7/17/2009 9:39:35 AM
Depressurize N2
7/17/2009 9:40:12 AM
Purge All to Resin
7/17/2009 9:40:19 AM
Transfer Resin to Reaction Vessel
7/17/2009 9:41:07 AM
Drain Filtered
7/17/2009 9:41:23 AM
Add DMF to Resin
7/17/2009 9:42:03 AM
Depressurize N2
7/17/2009 9:42:45 AM
Purge All to Resin
7/17/2009 9:42:51 AM
Add DCM to Resin
7/17/2009 9:43:40 AM
Depressurize N2
7/17/2009 9:44:16 AM
Purge All to Resin
7/17/2009 9:44:23 AM
Transfer Resin to Reaction Vessel
7/17/2009 9:45:11 AM
Drain Filtered
7/17/2009 9:45:27 AM
Add DMF to Resin
7/17/2009 9:46:06 AM
Depressurize N2
7/17/2009 9:46:48 AM
Purge All to Resin
7/17/2009 9:46:54 AM
Add DCM to Resin
7/17/2009 9:47:43 AM
Depressurize N2
7/17/2009 9:48:20 AM
Purge All to Resin
7/17/2009 9:48:26 AM
Transfer Resin to Reaction Vessel
7/17/2009 9:49:15 AM
Drain Filtered
7/17/2009 9:49:31 AM
Add Reagent: DMF
7/17/2009 9:50:14 AM
DMF (5.4/5.9)
7/17/2009 9:50:34 AM
Add Reagent: DCM
7/17/2009 9:50:38 AM
DCM (4.1/4.7)
7/17/2009 9:51:05 AM
Drain Filtered
7/17/2009 10:06:22 AM
Amino Acid: Gly
7/17/2009 10:07:00 AM
Amino Acid: Asn
7/17/2009 10:07:00 AM
Clean Resin Dip Tube: DMF
7/17/2009 10:07:01 AM
Wash - Cycle 1 of 1
7/17/2009 10:08:05 AM
DMF (5.8/5.9)
7/17/2009 10:08:30 AM
Add Reagent: Deprotect
7/17/2009 10:09:11 AM
Deprotect (5.0/0.0)
7/17/2009 10:09:43 AM
Microwave: Deprotection - Power: 35 Watts
7/17/2009 10:10:30 AM
Final Max Temp:31.4 C at end of test
7/17/2009 10:11:06 AM
Total Microwave Time: 0:36
7/17/2009 10:11:09 AM
Drain Filtered
7/17/2009 10:11:09 AM
Wash - Cycle 1 of 1
7/17/2009 10:11:45 AM
DMF (5.5/5.7)
7/17/2009 10:12:06 AM
Add Reagent: Deprotect
7/17/2009 10:12:46 AM
Deprotect (4.9/0.0)
7/17/2009 10:13:19 AM
Microwave: Deprotection - Power: 35 Watts
7/17/2009 10:14:07 AM
ACP
7/17/2009 9:35:03 AM
Started: