GE Sievers Innovox

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Current Mode Value

Continuous 0

Grab 1

Autosampler 2

Blank 3

Calibration 4

Verification 5

IC Calibration 6

Mock 7

Online 8

Check Standard 9

Rinse 10

Instrument Model Value

Laboratory 10

Online 20

Main Page

Identification Records3
- Table of Contents4
List of Tables10
List of Figures11
Revision History15
Confidentiality16
Declaration of Conformity17
Standard Limited Warranty17
- Limitation of Remedies and Liability18
- Limitación de Remedios y Responsabilidad18
- Limites de Correction et de Fiabilité18
- Beschränkte Ansprüche und Haftung18
- Limitazione DI Rimedi E Responsabilità19
- 限定責任および救済19
- 赔偿与责任限制19
Warnings20
Chapter 1: Introduction49
Chapter 2: System Description51
- System Specifications51
  - Additional System Specifications53
- Operating Specifications53
- Reagent Consumption54
- SCWO Method Compliance54
- System Overview54
- Sample Flow Path57
Sample Preparation Options61
- 2-Stream Configuration62
- Specifications - (2-Stream or 5-Stream) Clean Water Sampler62
- 2-Stream High Temperature Configuration62
- Specifications - (2-Stream) High Temperature Clean Water Sampler63
- Wastewater Sampler Option63
Chapter 3: Interferences67
- Safety67
- Reliability68
- Analytical Performance68
Chapter 4: Installation71
- Overview71
- Step 1: Unpack and Inspect the Analyzer71
  - Additional Installation Equipment73
- Step 2: Complete the Identification Records73
- Step 3: Select a Location for the Analyzer73
  - Mounting Stand Installation73
  - Wall Mount Installation77
- Step 4: Connect the Waste Lines77
- Step 5: Fill the Gas-Liquid Separator79
- Step 6: Install Input/Output, Cables, and Accessories79
The Gas-Liquid Separator79
Analog Outputs (TB1)81
Stream ID81
Alarm Outputs (TB3)82
- Table 5 Binary Input (TB2)82
Alarm Outputs (TB4)83
- Installing the 4-20 Ma Connection84
- Installing the Remote Start (Binary Input) Connection84
- Figure 9 Wiring Option - Binary Input Using Analyzer's External Supply85
- Installing the Analysis Complete Output Connection85
- Installing the Alarms and System Fault Output Connection86
- Installing the Ethernet Connection86
Figure 8 Wiring Option - Binary Input Using Analyzer's Internal Supply85
Connecting the Analyzer to a Computer86
- Installing the USB Connection87
Connecting the Analyzer to a Network87
- Step 7: Connecting to a Power Supply88
- Step 8: Connect the Sample Inlet System89
  - Installing the Online Sample System89
  - Installing the Wastewater Sampler90
    - To Install the Wastewater Sampler (Velocity Method)91
Figure 16 Top Wastewater Sampler Bracket W/Plate Adapter91
Velocity Method - Barb Fittings Identification92
- Figure 17: Lower Wastewater Sampler Bracket92
- Figure 20 Velocity Method - Adjusting the Sipper Tube Height93
- To Install the Wastewater Sampler (Overflow Method)94
Figure 19: Velocity Method - Installation93
Velocity Method - Failsafe Installation94
Figure 23 Top Wastewater Sampler Bracket W/Plate Adapter95
Lower Wastewater Sampler Bracket95
- Figure 25 Overflow Method - External Sample Pump Position96
- Figure 26 Overflow Method - Barb Fittings Identification96
- Figure 28 Overflow Method - Adjusting the Sipper Tube Height97
- Figure 27: Overflow Method - Installation97
- Installing the Check Standard System98
Overflow Method - Failsafe Installation98
- Installing the Grab Sample System99
- Step 9: Connect the Reagent and Dilution Water Lines99
- Step 10: Connect the Compressed Gas100
  - Installing the Carrier Gas Supply100
  - Installing the Gas Supply for the IP56 Accessory101
    - Specifications - IP56 Accessory102
- Step 11: Turn on Power and Configure Basic Settings102
  - Setting the Clock102
- Step 12: Perform a Test Analysis102
- Step 13: Calibrate the Analyzer104
Chapter 5: Calibration and Verification105
- Overview105
- Handling Standards106
  - Prepare IC Standard Solution106
- Calibration and Verification Options107
- Table 8 Maximum Dilution Allowed Using Auto Dilution Feature114
- Preparing for Calibration115
  - Save System Settings115
  - Perform Maintenance Tasks116
- Setting up NPOC, IC, TC/TOC Calibration116
- Calibrating the Analyzer118
Table 9 Approximate Number of Calibration Repetitions Possible118
Editing a Calibration119
- Editing a Calibration120
- Performing a Calibration Verification121
- Reviewing Calibration and Verification History122
Table 10 Approximate Number of Verification Repetitions Possible122
Chapter 6: Analyzer Operation123
- Overview123
  - The Main Screen123
  - Figure 38 the Main Screen (Grab Mode)124
- The Menu Screen125
  - Setting up Measurements (the Setup Tab)126
Figure 43 Operation with Five Streams and the Check Standard128
Configure Online Screen129
- Figure 44 Calculating the Run Time130
- Online Measurement-Configuration131
  - Operation with Multiple Streams131
- Figure 46: Stream 1 Screen132
- Check Standards134
Figure 47: Check Standard Setup Screen135
Check Standard (Setup) Screen137
- Clean Inlet138
- Auto Restart138
- Daily Flush138
- Summary139
- Grab Measurements139
  - Figure 51 the Grab (Setup) Screen140
  - Table 11 Vial Port - Repetitions Possible142
- Rinse143
- Measurement Settings143
Figure 52: the Maintenance Tab147
Configuring the Factor Units148
- Figure 54: Configuring the Factor Equation148
- Figure 56: Configuring the Factor Name149
- User Management150
  - Blank Correction150
  - Measuring the Blank151
The Data Screen152
- Viewing and Exporting Data152
  - Viewing Data on Screen152
  - Exporting Data152
Export (Data) Screen153
- Figure 60: Export Data Screen154
- Reviewing Exported Data155
Data Fields Output155
- Setting up Input and Output (I/O)156
Figure 65 Liquid Sensor Location - Hazardous Location Enclosure (ATEX or C1/D2)164
System Properties Screen166
- Setting the Clock167
- Upgrade Option167
- Gas Valve PID Parameters167
- Cleaning the Analyzer Screen168
- Setting the Fail Safe Option169
- Setting the Keyboard Options169
- Setting the Display Options169
- Archiving the Data History170
- Shutting down the Analyzer170
- Checking the Software Version171
Chapter 7: Operation with the Filter Panel173
- Operation of the Filter Panel with a Sample Pump173
- Control of Filter Panel173
Figure 69: Blowback Pulses and Sample Flow Time174
Flush/Blowback Screen175
Chapter 8: Maintenance177
- Recommended Spare Parts178
- Periodic Maintenance Tasks178
  - Periodic Inspections178
Consumables Replacement Schedule178
- Figure 72 Aging of 30% (W/V) Na 2 S 2 O 8 in HDPE Bottles179
- Preparing the Oxidizer Solution179
- Adding the Dilution Water180
- Performing a Flush180
- Preparing the Acid180
- Preparing the Persulfate Oxidizing Solution180
  - To Prepare the Oxidizing Solution180
- Cleaning the Analyzer181
- Cleaning the Gas-Liquid Separator181
- Figure 73 the Gas-Liquid Separator182
- Cleaning the Sparger183
The Sparger183
- Lubricating the Syringe184
Unscrewing the Syringe Base185
- Figure 75 Locating the Syringe Screw and Washers185
- Figure 77 Removing the Syringe186
- Figure 79 Removing the Stopper187
- Consumables Replacement188
- Other Maintenance Tasks193
Replacing the NDIR Filter193
- Replacing the High Pressure Valve Seals194
Figure 83: the High Pressure Valve Seal - before Removal195
The High Pressure Valve Seal - after Removal195
Table 15 2-Year Maintenance Worksheet - Sievers Innovox Online TOC Analyzer196
Chapter 9: Troubleshooting199
- Overview199
- Reviewing Warnings and Errors199
  - Analyzer Warnings and Error Messages200
- Other Software Errors210
The Diagnostics Screen217
- Valves218
  - Flow Control Valves218
The Flow Control Valve Screen218
- Figure 93 Sampler Handler Valves Screen219
- Gas Valves220
Diagnostic Result Screen220
- Gas Valve Testing Criteria221
- Pneumatic Valves222
Pneumatic Valve Screen222
- Heater223
  - Heater Testing Criteria224
- Ndir223
- Liquid Flow Check225
- Gas Leak Checks226
  - Figure 100 the Gas Leak Check Screen227
  - Figure 101 Gas Manifold Leak Check229
- Figure 102: Reactor Inlet Valve Leak Check231
- Figure 103: Reactor Bypass Leak Check233
- Figure 104 Reactor Leak Check235
- Figure 105 Reactor Outlet Valve Check237
- Leak Check238
- Analog Output239
- Binary Output239
- Binary Input240
- Figure 108 Binary Input Check241
- Pumps242
- Contacting Technical Support243
- Export Diagnostic Data243
- Testing the Sparger243
- Returning the Analyzer to GE Analytical Instruments244
Analyzer Dimensions (Front View)247
Appendix A: Analyzer Dimension Diagrams247
Analyzer Dimensions (Right Side View)248
Analyzer Dimensions (Left Side View)249
Appendix B: Acronyms and Definitions251
Appendix C: Importing Analyzer Data into a Spreadsheet255
- Importing Data into a Spreadsheet Program255
  - Figure 114 Microsoft Excel Spreadsheet Screen — Text Import Wizard - Step 1256
  - Figure 116 Microsoft Excel Spreadsheet Program — Text Import Wizard - Step 3257
Appendix D: Modbus Map259
Index265

GE Sievers Innovox - Page 263

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