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CBM-20A
Shimadzu CBM-20A User Manual
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5. Application Operation
5-74
CBM-20A/20A
lite
5.12.2 Autosampler
Comparison of Parameters for Dif
ferent Models
Parameter
SIL-
30ACMP
SIL-30AC
SIL-20A
SIL-
20AXR
SIL-20AC
SIL-
20ACXR
SIL-
10ADvp
SIL-10A
SIL-10AF
SIL-10AP
SIL-10Ai
SIL-10AXL
Method parameters
Rack
Needle S
troke
Needle S
troke (Ctrl)
Purge T
ime
Cooler
Cooler RackPlate L
Cooler RackPlate M
Cooler RackPlate R
Cooler T
emperature
Sampling Speed
Rinse V
olume
Rinse S
peed
Rinse Mode
Rinse Dip T
ime
Rinse T
ime
MTP T
ype
MTP Sample Order
MTP Tray
Needle S
troke
S
tack D
Needle S
troke
S
tack C
Needle S
troke
S
tack B
Needle S
troke
S
tack A
Sample Discharge
S
peed
Measuring Line
Purge V
olume
Air Gap V
olume
201
203
Table of Contents
Introduction
21
Default Chapter
3
CBM-20A Instruction Manual (Brief Manual
3
CBM-20A Instruction Manual (Detailed Manual) [PDF Instruction Manual
3
Model Names
3
Introduction
4
Warranty and After-Sales Service
5
Safety Instructions
7
Application Precautions
7
Installation Site Precautions
8
Operation Precautions
11
Precautions for Instrument Inspection, Maintenance, Adjustment and Care
12
Static Electricity Precautions
13
Typical Cause of Static Electricity Accidents
13
Preventing Static Electricity Accidents
14
In Case of Emergency
17
In Case of Power Outage
17
Maintenance, Inspections, and Adjustment
18
Precautions for Mobile Phase Selection and Use
19
Table of Contents
21
Chapter 1 Configuration
33
Overview
34
Features
34
Equipment Required for Connecting to the Network
35
Network Cables and Devices
35
Component Parts
37
Cbm-20A (S228-45012)
37
CBM-20Alite (S228-45011)
37
Optional Parts
38
Optical Cables
38
Optional Boards
38
RS-232C Cables
39
Chapter 2 Parts Identification and Function
42
Front Cover
42
Cbm-20A
42
Back
43
Cbm-20A
43
CBM-20Alite
44
Optional Parts
45
Back View of Optional Parts for CBM-20A
45
Applications and Windows
46
List of Windows
48
Group Monitor" Application
49
HPLC Explorer" Section
50
Status Summary" Section
51
Status" Tab Page
51
System Check" Tab Page
52
Maintenance" Tab Page
53
System Monitor" Section
54
Login" Window
56
Analysis Execution" Application
57
Analysis" Tab Page
58
Sequence" Section
59
Status Display
59
Method" Section
61
Monitor" Section
65
Configuration" Tab Page
67
Editing" Tab Page
68
Queue" Tab Page
69
Error" Window
71
Precautions Related to Internet Explorer Operations
72
Internet Explorer Settings
72
Popup Blocker
72
Entering and Confirming Parameter Settings
73
Out-Of-Range Data
73
Screen Printout
73
Continuous Operation
74
Message During Operation
74
Shortcut Keys
74
The Cache of Internet Explorer
74
Creating Shortcuts
75
Chapter 3 Preparation
78
Managing Several Systems as One Group
78
Managing Several Users
80
User Level
80
User Level and Access Level
80
Access Level
81
Starting the CBM-20A
82
Determine the System Configuration
83
Checking Connections between the System Controller and Components
85
Selecting the Pumping Mode
85
Selecting the Autosampler Control Method
87
Selecting the Fraction-Collector Control Method
87
Selecting the Unit-Name Allocation Method
87
Allocation with [Auto] Selected
88
Allocation with [Fixed] Selected
88
Making the Link Check Settings
89
Basic Operation
91
Chapter 4 Basic Operation
92
Overall Flow of Operation
92
Logging in and Displaying the "Analysis" Tab Page
93
Overall Flow of Operation
93
Starting Internet Explorer and Connecting to the CBM-20A
93
Starting the System Components
93
Selecting and Editing a Method File
94
Preparing Samples
95
Selecting and Editing a Sequence File
95
Executing Autopurge
96
Executing Analysis
98
Turning off the Solvent Delivery Module and Column Oven
98
Waiting for the System to Stabilize
98
Quitting Analysis
99
Quitting the System
99
Creating Method Files
100
Selecting Method Files
100
Creating Method Files
101
Buttons Common to "Method Parameter" and "Configuration Parameter" Windows
102
Displaying the "Method Parameter" Window
102
Editing the "Method Parameter" Window
102
Parameters for the Solvent Delivery Module
103
Selecting the Pressure Unit for the Pump
105
Parameters for the Autosampler
106
Parameters for the Column Oven
107
Parameters for the Detector
109
Parameters for the CBM-20A
110
Creating Sequence Files
112
Selecting Sequence Files
112
Creating Sequence Files
113
Creating Sequence Tables
116
Cutting and Copying
117
Editing Sequence Tables
117
Inserting, Pasting, or Inserting One Line
117
Gradient Analysis Using Time Programs
118
Displaying the "Time Program" Window
118
Creating Time-Program Tables
121
Time-Program Setting Example
123
Starting Analysis
124
Canceling "Cooling Down" or "Power down
124
Forcibly Stopping Analysis
124
Pausing Analysis Operation
124
Starting and Ending Analysis
124
Analysis Using a Manual Injector
125
Changing Parameters During Analysis
125
Starting Analysis
125
Printing Files
126
Printer
126
Print to Chromatopac
127
Printing Files
127
Chapter 5 Application Operation
130
Injecting Standard Samples at Regular Intervals
130
Example of Analysis Using Standard Sample Injection Table
130
Creating Standard-Sample Injection Tables
131
Setting the Mobile Phase Reserve Volume
133
Displaying the "Mobile Phase Reserve Volume Setting" Window
133
Checking the Mobile Phase Reserve Volume
135
Executing Autopurge for Solvent Delivery Modules and Autosamplers
137
Analysis Using Queues
138
Registering Sequence Files to the Analysis-Queue Tables
139
Deleting Registered Sequence Files
140
Displaying Analysis-Queue Tables
140
Editing Analysis-Queue Tables
140
Clearing Waiting Status
141
Clearing Waiting Status from the "Analysis" Tab Page
141
Clearing Waiting Status from the "Queue" Tab Page
141
Putting the Analysis Queue in Waiting Status
141
Starting Analysis
141
Shutdown and Startup Settings
142
Displaying the "Queue" Tab Page
142
Shutdown and Startup Parameters and Buttons
143
Advanced Shutdown Settings" Window
144
Advanced Startup Settings" Window
146
Analysis Using Fraction Collectors
149
Parameters for the Fraction Collector
149
Selecting Method Files
149
Controlling the Fraction Collector with a Time Program
150
Displaying the "Fraction Collector Rack Adjustment" Window
150
Setting the Number and Positions of Vials in Racks
150
Functions of Buttons
151
Adjusting the Rack Position
152
Managing Files
153
Saving Files to a PC
153
Creating New Files Using Existing Files
156
Downloading Files from a PC
157
Managing Component Parameters
161
Saving All Component Parameters to a PC
161
Downloading All Component Parameters from a PC
163
Initializing Parameters
165
Managing Groups
167
Displaying the "Group Settings" Application Window
167
Group Information" Tab Page
169
Sharing and Centralizing User Information for Systems in a Group
170
System Administration" Tab Page
171
Advanced Settings" Window
172
Changing System Names
173
Moving Systems to Different Groups
174
Creating New Groups
175
User Registration
176
Registering New Users
177
Changing User Information
180
Deleting User Information
180
User Levels and Functions
181
Changing Passwords
183
Locking Systems
184
Parameter Details
185
Pump
185
Autosampler
202
Autosampler
208
Detector
224
Hardware Validation
299
Overview of Hardware Validation
300
Implementation of Hardware Validation
301
Validation Precautions
302
Equipment Required for Validation
305
Validation: System Controller
307
System Validation
310
If Validation Fails
321
Technical Information
337
Installation
338
Connecting the System Controller and Components
343
Initializing Components
365
System Controller Installation and Setup (Example)
368
Specifications
379
Maintenance Parts
388
Introduction to HPLC System
389
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Shimadzu CBM-20A Specifications
General
Brand
Shimadzu
Model
CBM-20A
Category
Controller
Language
English
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