xiv July 29, 2013, 715003794 Rev. B
Enter values in parameter fields ...................................................................... 88
Configure the separations module ................................................................ 91
Set configuration parameters............................................................................ 91
Configure the operating mode........................................................................... 98
Prepare the solvent management system .................................................. 103
Prepare solvent reservoirs............................................................................... 104
Degassing solvents........................................................................................... 105
Prime the plunger seal-wash pump................................................................ 106
Prime the solvent management system.......................................................... 107
Prepare the sample management system for operation ......................... 107
Purge the system ............................................................................................. 108
Prime the needle-wash pump.......................................................................... 109
Adjust the seal pack......................................................................................... 110
Load carousels.................................................................................................. 111
Procedures for preparing the separations module for operation ........ 112
Prepare a new or dry separations module for operation ............................... 112
Prepare an idle or powered-off separations module for operation ................ 113
Change from a buffered solvent to an organic solvent................................... 114
Power-off the separations module ............................................................... 114
Flush the flow path.......................................................................................... 115
Power-off the separations module................................................................... 115
4 Front Panel Control ............................................................................. 117
Routine startup ................................................................................................ 117
Reinitialize the system .................................................................................... 118
Load sample vials ............................................................................................. 118
Remove the carousel ........................................................................................ 118
Load vials ......................................................................................................... 118
Load the carousel............................................................................................. 119
Add new sample vials during a run................................................................ 119
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