HTA HT2800T - Page 255

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• Pre-extraction: Before extraction, in this case the Fiber is exposed to the derivatizing agent and

then it is exposed to the sample to be analyzed, in this way the analytes are extracted and

simultaneously converted into molecules with greater affinity for the Fiber.

Main Page

Table of Contents3
Introduction9
Intended Use and Restrictions9
Symbol Table10
Warning11
Standards Compliance14
General Specification14
Functions Available Only through15
Hta Autosampler Manager15
Vial Leakage Check (Headspace Mode)15
Method Development Option (Headspace Mode)15
Versions15
Description15
Options16
Technical Specifications17
PC Software Requirements (HTA Autosampler Manager)20
Equipment Description21
Parts Definition21
HT2800T/HT2850T Overview21
Syringe Location27
Connection Panel35
Moving Parts36
Tool Kit37
Touch Screen Display Description38
Touchscreen Use38
Limited Warranty42
Installation44
Unpacking and Preliminary Operations44
Autosampler Assembly45
How to Lift and Carry the Autosampler49
Installation49
Autosampler Installation on the Mounting Plate51
Safety Lock Setting56
Electrical Connections57
Purge Line Connections (for Headspace and Fiber Cleaning Device)58
Preparing the Solvent and Waste Vials (Liquid Mode)/ Preparing the Washing Vial (SPME Mode)59
Start-Up60
Pc Connection and Software Installation61
Autosampler Controlled by LAN-Connected PC61
Autosampler Connected Directly to the PC70
Accessories Installation71
External Pressure Regulator Installation (Only for Headspace and SPME Mode)71
Swagelok Adapter Installation (Only Forheadspace and SPME Mode)72
System Integrity Tool Installation (Only for Headspace Mode)73
Vial Locator: Installing and Removing (Liquid Mode)75
Preparing Sample Vial78
Vial Filling in Liquid Mode79
Vial Capping (Screw Cap)79
Vial Capping (Crimping Cap)79
Final Installation Operations83
Basic Training83
Set up Operations84
View Parameters84
Setup85
Setup: Alignment85
Setup: Syringe Warmer Assembly Installation/ Replacement (Headspace Mode)92
Syringe Installation/ Replacement (Liquid Mode)101
SPME Fiber Holder Installation/ Replacement111
Setup: Manual Operations119
Setup: Configuration123
Setup: Service135
Programming Method136
Method (Headspace Mode)136
Method Menu136
Method X: Setting Method Parameters136
Method Tools140
Example140
Method (Liquid Mode)141
Method Menu141
Method X: Setting Method Parameters142
Method Tools146
Example146
Method: SPME Mode147
Method Menu147
Method X: Setting Method Parameters147
Method Tools153
Example153
Programming Sequence155
Sequence: Headspace Mode155
Sequence Menu155
Setting Sequence Step Parameters155
Sequence Tools156
Sequence: Liquid Mode157
Sequence Menu157
Setting Sequence Step Parameters157
Sequence Tools159
Sequence: SPME Mode159
Sequence Menu159
Setting Sequence Step Parameters160
Sequence Tools161
Operations162
Home Screen162
Home Screen: Standard User Interface162
Home Screen: Quick Start User Interface164
Single Injection165
Automatic Run166
Interrupting an Automatic Run167
Immediate Injection167
Skip Next Vial Option167
Priority Injection168
Syringe Purge169
Syringe Wash169
Fiber Cleaning/Conditioning170
Load and Unload Sample Vial170
Load and Unload Solvent Vials171
Settings Menu171
Change Tray/Rack Type171
Eco Savings173
Change Mode174
Change from Headspace to Liquid Mode175
Change from SPME to Liquid Mode182
Change from Liquid to Headspace Mode189
Change from Liquid to SPME Mode195
Change from Headspace to SPME Mode201
Change from SPME to Headspace Mode204
Troubleshooting207
Introduction207
Start up Errors208
Safety Lock Error208
Vial Locator Error208
Memory Error209
Method Errors209
Fill Volume/Pull up Strokes Setting Incompatibility209
Fill Volume/Syringe Pre-Fill Setting Incompatibility210
Internal Standard Setting Error210
Sample Washes" Setting Error211
Touch Sensor Problems211
Falling Vials211
Obstacle Found212
Obstacle Found During Cover Movement213
Lack of a Vial (Waste or Solvent Vial for Liquid Mode, Washing Vial for SPME Mode)213
Mismatch Errors214
Syringe Wash Mismatch Error214
Single Injection Mismatch Error214
Automatic Run Mismatch Errors215
Missing Errors217
Missing: Rear Injector Alignment217
Timeout Error218
Peripheral Communication Timeout218
Syringeid Timeout218
Mechanical Errors219
Heating Errors219
System Integrity Test Fail220
Damage to Syringe Needle220
Syringe Inspection221
Tray Emergency Release222
Tray Opening by Hand222
HTA Autosampler Manager" Troubleshooting224
Autosampler and PC Do Not Communicate (Connection by LAN)224
Analytical Troubleshooting226
Analytical Troubleshooting (Headspace Mode)226
Analytical Troubleshooting (Liquid Mode)228
Bar Code Reader Troubleshooting230
Maintenance232
Ordinary Maintenance232
Cleaning of Vial Rack/Tray232
External Cleaning of Cabinet233
Incubation Oven Cleaning233
Touch Screen Display Cleaning234
Syringe Replacement in the Syringe Warmer Assembly (Headspace Mode)234
Fiber Replacement in the Fiber Holder (SPME Mode)241
Septum of the System Integrity Tool Replacement (Headspace Mode)243
Preventive Maintenance Pack243
Extraordinary Maintenance244
Uninstalling and Disposal245
Autosampler Uninstalling245
Autosampler Shipping246
Autosampler Disposal250
Disposal Instructions251
Appendix A - Glossary252
Headspace Mode252
Liquid Mode253
Spme Mode254
Appendix B - Consumables256
Consumables for Headspace Mode256
Syringes256
Sample Vials256
Consumables for Liquid Mode260
Syringes260
Sample Vials263
Solvent and Waste Vials266
Consumables for Spme Mode266
Fibers266
Washing Vial266
Appendix C - Analyzer Connector267
RS232C Interface (Optional)269

HTA HT2800T - Page 255

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