Table of Contents xv
Installing the GC column ................................................................................ 6-9
Configuring the GC and autosampler ........................................................ 6-11
Removing the GC interface .......................................................................... 6-11
7 The Direct Insertion Probe .................................................................. 7-1
Introduction ....................................................................................................... 7-2
Installing the probe insertion lock ............................................................... 7-2
Inserting and removing the DI probe .......................................................... 7-4
Loading sample into the DI probe................................................................... 7-4
Inserting the DI probe into the insertion lock................................................ 7-6
Removing the DI probe from the probe insertion lock................................... 7-8
Controlling the DI probe temperature ...................................................... 7-10
Ramping the probe temperature manually.................................................. 7-10
Ramping the probe temperature automatically........................................... 7-11
Probe Control dialog box Ramps tab............................................................. 7-14
Probe Control dialog box ............................................................................... 7-16
Ramping the probe during a acquisition ...................................................... 7-17
8 The Direct Chemical Ionization (DCI) Probe .................................. 8-1
Introduction ....................................................................................................... 8-2
Installing the probe insertion lock ............................................................... 8-2
Inserting and removing the DCI probe ....................................................... 8-3
Loading sample into the DCI probe................................................................ 8-3
Inserting the DCI probe into the insertion lock............................................. 8-4
Removing the DCI probe from the probe insertion lock................................ 8-6
Controlling the DCI probe current ............................................................... 8-7
Ramping the probe current manually ............................................................ 8-7
Ramping the probe current automatically ..................................................... 8-8