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ACCUPYC II 1345
Micromeritics ACCUPYC II 1345 User Manual
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6
Perform
an
Analy
s
i
s
6
-
4
Acc
uPyc
II
134
5
O
perat
or
Manu
al
134
-428
51-01
(R
ev
A
)
—
Jan
2021
87
89
Table of Contents
Default Chapter
4
Corporate Profile
4
Contact Us
5
About this Manual
6
General Safety
7
Table of Contents
10
1 About the Accupyc
17
Instrument Components
19
About the TEC Module
20
Asphalt Density Application
21
About the Foampyc Module
21
Equipment Options and Upgrades
23
Configuration Options
24
Gas Requirements
26
Specifications for Accupyc
27
Specifications for Accupyc II TEC
31
2 Data Entry with Keypad
33
About the Display
34
About the Keypad
35
System Commands
38
Cancel an Analysis
40
Manual Mode
41
Transmit Data
42
Analysis Parameters
42
Review Data
45
View Data Results
47
Print a File
47
3 About the Software
49
Menu Structure
49
Common Fields and Buttons
50
Option Presentation
53
File Status
55
Keyboard Shortcuts
56
Default Methods
57
Analyzer Status
58
Show Instrument Log
58
Show Instrument Schematic
59
Show Status
61
Export Files
62
List Files
62
Open a Sample File
63
Software Updates
64
Reinstall or Modify the Software
65
Software Uninstall
66
Unit Selection
66
Software in 21CFR11 Environments
67
Option Presentation for 21CFR11 Environments
69
Uninstall Software in 21CFR11 Environments
71
4 Sample Files
73
Create Sample Files
73
Sample Cup
77
Material Parameters
78
5 Parameter Files
79
Analysis Conditions
80
Report Options
83
6 Perform an Analysis
85
Prepare and Load a Sample
85
Perform an Analysis Using the Software
87
Perform an Analysis Using the Keypad
89
Quickstart Analysis
91
Sequence Analysis
92
Review Analysis
93
7 About Reports
95
Open and Close Reports
95
Start Reports
95
SPC Report
96
Report Features and Shortcuts
100
Graph Features and Shortcuts
105
Graph and Sample Overlays
109
Generate Multiple Graph Overlays
109
Generate Multiple Sample Overlays
111
Report Examples for Pycnometry Analyzers
113
Combined Report
113
Summary Report
114
Tabular Report
115
Graph Report
116
Overlay Report
117
Equilibration Report
118
Sample Log Report
119
8 Selected Reports
121
Combined Report
121
Density and Volume Table
122
Density Volume Vs Cycle Number Trend Plot
123
Density Vs Time Trend Plot
125
Equilibration Report
126
Options Report
128
Pressure and Volume Table
128
Sample Log Report
129
Summary Report
129
Total Pore Volume Vs Temperature
130
Volume Vs Cycle Number Trend Plot
131
9 Diagnostics Using the Software
133
10 About Calibration
135
Calibrate Using the Software
135
Calibrate Pressure Scale
135
Calibration Report
136
Calibrate Temperature Offset
137
Calibrate Zero Cell Volume
138
Calibrate Zero Pressure
139
Reset Pressure Calibration
140
Calibrate Volume Scale
141
Verify Operation
145
Load Calibration from File
147
Save Calibration to File
147
Calibrate Using the Keypad
148
Calibrate Function
148
Calibration Data
149
Calibrate Volume
150
Reset Pressure Calibration
151
Review Calibration
152
Calibrate Temperature
154
Zero the Pressure Transducer & Chamber Volume
154
Load Calibration Data from a USB Media
155
Copy Calibration Data to a USB Media
155
11 Hardware
157
Add Analysis Module to Control Module
157
Analytical Balance
159
Brightness Control
160
Handling System Components
161
RS232 Pin Assignment
162
12 Maintenance and Troubleshooting
163
Power
166
Chamber Cap O-Ring
167
Check the Cell and Expansion Chambers for Leaks
169
Clean the Dust Filter
171
Clean the Pycnometer
172
Decontamination of the Pycnometer
172
Guidelines for Connecting Gases
173
Replace a Gas Cylinder
174
Regulator Pressure
177
Recover from a Power Failure
179
Reset the Pycnometer
179
Power Instrument on and off
180
Service Test Mode
181
Parts Replacement
181
13 TEC Module
183
Set the TEC Temperature
183
Operate the TEC Module
184
Volume Change with Temperature for the 100 Cm3 Accupyc
185
Asphalt Density Measurement
186
14 Temperature-Controlled Accupyc
187
Attach a Circulating Bath
187
Add Analysis Modules to a Temperature Controlled Module
188
15 Multivolume Insert Option
189
16 Multigas Option
195
A Advanced Reports - Python Module a
197
Advanced Report Options a
198
Graphic Reports a
199
Add a Curve a
199
Add a Curve Using the Second Y-Axis
200
Create a New Graphical Report
201
Scripts a
202
Run a Script a
202
Remove a Script a
202
Edit a Script a
203
Python Reports a
204
Graphic Report a
204
Summary Report a
205
Tabular Report a
206
Enable the Use of Overlay Data a
207
Summary Reports a
210
Graphic Reports a
211
Get Sample Information Item a
213
B Exported Data Example B
215
C Sample Volume Equation Derivation C
221
D Transmitted Data D
225
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Micromeritics ACCUPYC II 1345 Specifications
General
Brand
Micromeritics
Model
ACCUPYC II 1345
Category
Measuring Instruments
Language
English
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