Milestone Srl MA245-003 – ultraWAVE 3 – User Manual
5
Acid mixtures ................................................................... 55
Addition of Reagents ........................................................ 57
Addition of base load in the main PTFE vessel ................... 57
Handling of sample rack ................................................... 59
Locking of clamps ............................................................ 60
Pressure load before the microwave run ............................ 61
Microwave run ................................................................. 62
Pressure release after microwave run ................................ 62
Opening of reactor after digestion run ............................... 63
System status indicator .................................................... 64
Emergency Stop of UltraWAVE 3 ....................................... 65
9 MAINTENANCE AND CLEANING PROCEDURES
67
Cleaning after each run .................................................... 67
Cleaning of reactor and checking of the main PTFE vessel .......................... 67
Cleaning of reactor and cover with protective oil and grease
69
How to apply the PFPE grease with anticorrosion additive........................... 70
NOx decontamination of the main PTFE vessel .................. 71
Cleaning before long operational Breaks ............................ 71
Cleaning of the metal cover .............................................. 72
Cleaning instructions in case of spilt acids ......................... 73
Vessel Covering ............................................................... 75
Leak Test of the main reactor ........................................... 75
Measures in case of fast pressure release .......................... 76
Maintenance of High-pressure compressor (optional) ......... 76
Check Oil Level ....................................................................................... 76
Condensate draining................................................................................ 77
10 EASYCONTROL SOFTWARE............................ 78
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