Operation Manual 235
17 Chromatographic Checkout
About Chromatographic Checkout 236
To Prepare for Chromatographic Checkout 237
To Check FID Performance 239
To Check TCD Performance 244
To Check NPD Performance 248
To Check ECD Performance 252
To Check FPD+ Performance (Sample 5188-5953) 256
Preparation 256
Phosphorus performance 256
Sulfur performance 260
To Check FPD+ Performance (Sample 5188-5245, Japan) 262
Preparation 262
Phosphorus performance 262
Sulfur performance 266
This section describes the general procedure for verifying performance against the original
factory standards. The checkout procedures described here assume a GC that has been in use
for some period of time. Therefore the procedures ask that you perform bakeouts, replace
consumable hardware, install the checkout column, and so forth.
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