15 Inletsï€
212 Operation Manual
Selecting the correct MMI liner
Split liner
A good liner for split mode operation will offer very little restriction to the split flow path
between the bottom of the liner and the inlet body and between the outside of the liner and the
inside of the inlet body. The preferred Agilent split liner, part number 5183-4647, incorporates a
glass positioning bead on the bottom to facilitate this. It will also incorporate glass wool or
some other source of surface area inside the liner that provides for complete sample
vaporization across the boiling point range of the sample. Select an appropriate liner from
Table 29.
Splitless liner
The liner volume must contain the solvent vapor. The liner should be deactivated to minimize
sample breakdown during the purge delay. Solvent vapor volume can be reduced by using
Pulsed Splitless mode. Use the Vapor Volume Calculator to determine vapor volume
requirements.
Vapor volume < 300 µL Use 2 mm liner (250 µL volume), 5181-8818 or similar.
Vapor volume 225 – 300 µL Consider pulsed splitless mode to reduce vapor volume.
Vapor volume > 300 µL Use 4 mm liner, 5062-3587 or similar.
Vapor volume > 800 µL Consider pulsed splitless mode to reduce vapor volume.
For thermally labile or reactive samples, use G1544-80700 (open top) or G1544-80730 (top
taper) liners.
Table 29 Split mode liners
Liner Description Volume Mode Deactivated Part Number
Low Pressure Drop –
Positioning Bead
870 µL Split – Fast
Injection
Yes 5183-4647
4mm ID, Glass Wool 990 µL Split – Fast
Injection
No 19251-60540
Empty Pin & Cup 800 µL Split – Manual
Only
No 18740-80190
Packed Pin & Cup 800 µL Split – Manual
Only
No 18740-60840
Table 30 Splitless mode liners
Liner Description Volume Mode Deactivated Part Number
Single Taper Glass
Wool
900 uL Splitless Yes 5062-3587
Single Taper 900 uL Splitless Yes 5181-3316