Agilent Technologies 8890 - Page 245

17 Chromatographic Checkout
Operation Manual 245
Multimode inlet
Mode Splitless
Inlet temperature 40 °C
Initial time 0.1 min
Rate 1 720 °C/min
Final temp 1 350 °C
Final time 1 2 min
Purge time 1.0 min
Purge flow 40 mL/min
Septum purge 3 mL/min
Purged packed column inlet
Temperature 250 °C
Septum purge 3 mL/min
Cool on-column inlet
Temperature Oven track
Septum purge 15 mL/min
PTV inlet
Mode Splitless
Inlet temperature 40 °C
Initial time 0.1 min
Rate 1 720 °C/min
Final temp 1 350 °C
Final time 1 2 min
Rate 2 100 °C/min
Final temp 2 250 °C
Final time 2 0 min
Purge time 0.5 min
Purge flow 40 mL/min
Septum purge 3 mL/min
Detector
Temperature 300 °C
Reference flow (He) 30 mL/min
Makeup flow (He) 2 mL/min
Baseline output < 30 display counts on Agilent OpenLAB CDS
ChemStation Edition (< 750 µV)
Table 43 TCD Checkout Conditions (continued)