Agilent Technologies 8890 - Page 241

17 Chromatographic Checkout
Operation Manual 241
PTV inlet
Mode Splitless
Inlet temperature 75 °C
Initial time 0.1 min
Rate 1 720 °C/min
Final temp 1 350 °C
Final time 1 2 min
Rate 2 100 °C/min
Final temp 2 250 °C
Final time 2 0 min
Purge time 0.5 min
Purge flow 40 mL/min
Septum purge 3 mL/min
Detector
Temperature 300 °C
H2 flow 30 mL/min
Air flow 400 mL/min
Makeup flow (N2) 25 mL/min
Lit offset Typically 2 pA
Oven
Initial temp 75 °C
Initial time 0.5 min
Rate 1 20 °C/min
Final temp 190 °C
Final time 0 min
Table 42 FID Checkout Conditions