17 Chromatographic Checkout
250 Operation Manual
7 If using a data system, prepare the data system to perform one run using the loaded
checkout method. Make sure that the data system will output a chromatogram.
8 Start the run.
If performing an injection using an autosampler, start the run using the data system, or
creating a one sample sequence and pressing on the touchscreen.
If performing a manual injection (with or without a data system):
a Select to prepare the inlet for splitless injection.
Oven
Initial temp 60 °C
Initial time 0 min
Rate 1 20 °C/min
Final temp 200 °C
Final time 3 min
ALS settings (if installed)
Sample washes 2
Sample pumps 6
Sample wash volume 8 (maximum)
Injection volume 1 µL
Syringe size 10 µL
Solvent A pre washes 2
Solvent A post washes 2
Solvent A wash volume 8
Solvent B pre washes 0
Solvent B post washes 0
Solvent B wash volume 0
Injection mode (7693A) Normal
Airgap Volume (7693A) 0.20
Viscosity delay 0
Inject Dispense Speed (7693A) 6000
PreInjection dwell 0
PostInjection dwell 0
Manual injection
Injection volume 1 µL
Data system
Data rate 5 Hz
Table 44 NPD Checkout Conditions (continued)
To Next Page
Loading...
